2,4-DINITROBENZENESULFONYL CHLORIDE

Mass

MS-NW-6488          
2,4-dinitrobenzenesulfonyl chloride
C6H3ClN2O6S         (Mass of molecular ion:    266)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       1.5
      18.0       7.3
      28.0       3.8
      30.0      45.0
      36.0       3.0
      37.0       2.1
      38.0       5.1
      39.0       2.4
      45.0       1.9
      46.0       4.6
      48.0       7.7
      49.0       1.1
      50.0       4.1
      51.0       3.8
      53.0       2.9
      61.0       1.8
      62.0       5.8
      63.0      15.1
      64.0      20.7
      66.0       1.0
      69.0       1.6
      73.0       3.0
      74.0      21.0
      75.0      35.2
      76.0       4.9
      77.0       3.0
      79.0       8.9
      84.0       1.8
      86.0       1.1
      91.0       2.8
      92.0       1.2
      93.0       6.4
      98.0       1.5
     107.0       1.8
     109.0       7.2
     110.0       9.0
     111.0       3.4
     112.0       3.2
     126.0       2.5
     140.0       1.2
     156.0       1.2
     168.0       2.3
     202.0      10.7
     204.0       4.1
     214.0       1.9
     231.0     100.0
     232.0       8.3
     233.0       6.2
     266.0       2.7
     268.0       1.2
     288.0       3.3

Assign. Shift(ppm) A 8.70 B 8.66 C 8.51 J(A,B)=2.0HZ. J(B,C)=9.1HZ.

     Hz     ppm     Int.

    783.13   8.745     59
    781.13   8.722    390
    780.00   8.710    562
    777.94   8.687    552
    775.94   8.664     44
    774.00   8.643    705
    771.88   8.619    408
    770.00   8.598     31
    769.63   8.594     30
    765.31   8.546   1000
    762.88   8.519     37
    762.13   8.510     69
    759.25   8.478     66
    756.06   8.442    308