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50892-23-4

WY-14643

Product Name WY-14643

CAS50892-23-4

MFC14H14ClN3O2S

MW323.8

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  • 50892-23-4_ms
    Mass

    MS-IW-4918          
    (4-chloro-6-(2,3-xylidino)-2-pyrimidinylthio)acetic acid
    C14H14ClN3O2S       (Mass of molecular ion:    323)
    

       Source Temperature: 180 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          17.0       1.0
          18.0       5.0
          27.0       2.5
          28.0       1.7
          35.0       1.2
          36.0       7.9
          38.0       2.5
          39.0       3.9
          41.0       1.4
          42.0       1.2
          43.0       1.5
          44.0       3.9
          45.0       2.7
          46.0       1.7
          47.0       1.1
          51.0       3.6
          52.0       1.9
          53.0       2.4
          63.0       1.9
          64.0       1.0
          65.0       3.8
          70.0       1.1
          77.0      16.5
          78.0       4.3
          79.0       9.1
          89.0       1.7
          90.0       1.1
          91.0       6.3
          92.0       2.0
          93.0       1.2
         102.0       2.0
         103.0       8.0
         104.0       2.9
         105.0       8.7
         106.0       5.8
         107.0       1.2
         109.0       2.3
         115.0       2.7
         116.0       2.2
         117.0       2.4
         118.0       2.3
         119.0       1.5
         120.0       4.9
         120.5       1.7
         121.0       1.6
         128.0       1.5
         129.0       1.4
         130.0       4.2
         131.0       3.8
         132.0       1.7
         138.5       3.4
         139.0       1.0
         139.5       1.6
         140.0       1.5
         142.0       4.3
         143.0       3.7
         144.0       9.0
         145.0       5.3
         154.0       1.1
         155.0       3.9
         156.0       2.8
         157.0       1.4
         162.0       2.4
         168.0       1.6
         169.0      10.7
         170.0       6.8
         171.0       7.3
         172.0       2.2
         178.0       1.6
         180.0       1.6
         181.0       1.1
         182.0       1.7
         183.0       2.5
         184.0       1.9
         185.0       2.0
         196.0       2.5
         197.0       2.4
         198.0       6.6
         199.0       1.3
         201.0       4.1
         202.0       1.1
         203.0       1.6
         205.0       1.6
         207.0       1.2
         214.0       1.0
         216.0       1.4
         217.0       2.0
         218.0       6.7
         219.0       2.9
         220.0       2.3
         226.0       1.5
         228.0      14.5
         229.0       2.8
         230.0       3.3
         231.0       1.6
         232.0      11.1
         233.0       4.6
         234.0       4.4
         235.0       1.6
         240.0       1.0
         242.0       1.8
         244.0       3.5
         245.0       1.8
         246.0      17.1
         247.0       3.1
         248.0       6.5
         249.0       2.1
         250.0       1.9
         262.0       2.9
         263.0       1.8
         264.0     100.0
         265.0      15.6
         266.0      37.2
         267.0       5.6
         268.0       2.0
         269.0       1.2
         270.0       1.3
         272.0       1.8
         274.0       1.1
         276.0       2.3
         277.0       2.8
         278.0       8.1
         279.0       9.1
         280.0       4.2
         281.0       3.2
         287.0       2.4
         288.0       1.1
         305.0       7.8
         306.0       2.0
         307.0       3.2
         308.0       1.3
         322.0       1.9
         323.0      20.2
         324.0       4.3
         325.0       7.9
         326.0       1.3
    

400 MHz in DMSO-d6

  • 50892-23-4_1hnmr

    1H NMR 399.65 MHz
    C14 H14 Cl N3 O2 S 0.040 g : 0.5 ml DMSO-d6
    (4-chloro-6-(2,3-xylidino)-2-pyrimidinylthio)acetic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.7 B 9.49 C 7.13 to 7.10 D 6.2 E 3.840 F 2.276 G 2.076

         Hz     ppm     Int.
    

       5085.98  12.727     59
       3791.91   9.489     61
       2851.54   7.136    159
       2848.97   7.129    130
       2844.94   7.119    213
       2838.16   7.102    138
       2830.29   7.082     28
       2829.92   7.081     28
       1535.12   3.842    188
        910.15   2.278    929
        829.74   2.077   1000
    

in DMSO-d6

  • 50892-23-4_13cnmr

KBr disc

  • 50892-23-4_ir1_2

nujol mull

  • 50892-23-4_ir2