WY-14643

Mass

MS-IW-4918          
(4-chloro-6-(2,3-xylidino)-2-pyrimidinylthio)acetic acid
C14H14ClN3O2S       (Mass of molecular ion:    323)

   Source Temperature: 180 °C
   Sample Temperature: 180 °C
   Direct, 75 eV

      17.0       1.0
      18.0       5.0
      27.0       2.5
      28.0       1.7
      35.0       1.2
      36.0       7.9
      38.0       2.5
      39.0       3.9
      41.0       1.4
      42.0       1.2
      43.0       1.5
      44.0       3.9
      45.0       2.7
      46.0       1.7
      47.0       1.1
      51.0       3.6
      52.0       1.9
      53.0       2.4
      63.0       1.9
      64.0       1.0
      65.0       3.8
      70.0       1.1
      77.0      16.5
      78.0       4.3
      79.0       9.1
      89.0       1.7
      90.0       1.1
      91.0       6.3
      92.0       2.0
      93.0       1.2
     102.0       2.0
     103.0       8.0
     104.0       2.9
     105.0       8.7
     106.0       5.8
     107.0       1.2
     109.0       2.3
     115.0       2.7
     116.0       2.2
     117.0       2.4
     118.0       2.3
     119.0       1.5
     120.0       4.9
     120.5       1.7
     121.0       1.6
     128.0       1.5
     129.0       1.4
     130.0       4.2
     131.0       3.8
     132.0       1.7
     138.5       3.4
     139.0       1.0
     139.5       1.6
     140.0       1.5
     142.0       4.3
     143.0       3.7
     144.0       9.0
     145.0       5.3
     154.0       1.1
     155.0       3.9
     156.0       2.8
     157.0       1.4
     162.0       2.4
     168.0       1.6
     169.0      10.7
     170.0       6.8
     171.0       7.3
     172.0       2.2
     178.0       1.6
     180.0       1.6
     181.0       1.1
     182.0       1.7
     183.0       2.5
     184.0       1.9
     185.0       2.0
     196.0       2.5
     197.0       2.4
     198.0       6.6
     199.0       1.3
     201.0       4.1
     202.0       1.1
     203.0       1.6
     205.0       1.6
     207.0       1.2
     214.0       1.0
     216.0       1.4
     217.0       2.0
     218.0       6.7
     219.0       2.9
     220.0       2.3
     226.0       1.5
     228.0      14.5
     229.0       2.8
     230.0       3.3
     231.0       1.6
     232.0      11.1
     233.0       4.6
     234.0       4.4
     235.0       1.6
     240.0       1.0
     242.0       1.8
     244.0       3.5
     245.0       1.8
     246.0      17.1
     247.0       3.1
     248.0       6.5
     249.0       2.1
     250.0       1.9
     262.0       2.9
     263.0       1.8
     264.0     100.0
     265.0      15.6
     266.0      37.2
     267.0       5.6
     268.0       2.0
     269.0       1.2
     270.0       1.3
     272.0       1.8
     274.0       1.1
     276.0       2.3
     277.0       2.8
     278.0       8.1
     279.0       9.1
     280.0       4.2
     281.0       3.2
     287.0       2.4
     288.0       1.1
     305.0       7.8
     306.0       2.0
     307.0       3.2
     308.0       1.3
     322.0       1.9
     323.0      20.2
     324.0       4.3
     325.0       7.9
     326.0       1.3

Assign. Shift(ppm) A 10.7 B 9.49 C 7.13 to 7.10 D 6.2 E 3.840 F 2.276 G 2.076

     Hz     ppm     Int.

   5085.98  12.727     59
   3791.91   9.489     61
   2851.54   7.136    159
   2848.97   7.129    130
   2844.94   7.119    213
   2838.16   7.102    138
   2830.29   7.082     28
   2829.92   7.081     28
   1535.12   3.842    188
    910.15   2.278    929
    829.74   2.077   1000