Tetramisole hydrochloride

Mass

MS-NW-9395          
(+-)-6-phenyl-2,3,5,6-tetrahydroimidazo(2,1-b)thiazole hydrochloride
C11H12N2S HCl       (Mass of molecular ion:    204)

   Source Temperature: 220 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       1.1
      18.0       2.7
      27.0       3.8
      28.0       6.6
      29.0       1.6
      30.0       1.4
      35.0       3.2
      36.0      33.1
      37.0       1.1
      38.0      10.7
      39.0       4.7
      41.0       2.6
      42.0       3.1
      45.0       8.8
      46.0       1.1
      50.0       2.8
      51.0       7.5
      52.0       1.8
      54.0       3.2
      55.0       1.3
      56.0       7.9
      59.0       2.4
      60.0       2.6
      61.0       1.2
      62.0       1.3
      63.0       4.6
      64.0       1.6
      65.0       3.0
      69.0       1.9
      71.0       1.1
      72.0       5.1
      73.0      60.8
      74.0       3.6
      75.0       3.8
      76.0       2.3
      77.0      12.3
      78.0       3.9
      88.0       1.9
      89.0       7.7
      90.0       3.8
      91.0       6.3
      98.0       2.0
      99.0       3.2
     100.0       1.5
     101.0      59.6
     102.0       6.6
     103.0       9.6
     104.0      15.3
     105.0       1.7
     115.0       1.1
     116.0       3.2
     117.0       6.5
     118.0       2.4
     121.0      13.1
     122.0       2.3
     126.0       2.9
     127.0      18.9
     128.0       2.2
     129.0       1.3
     130.0       1.4
     131.0       2.0
     143.0       1.1
     144.0       1.9
     148.0      87.2
     149.0      10.3
     150.0       4.6
     175.0       1.3
     176.0       5.9
     177.0       1.0
     202.0       2.6
     203.0      34.2
     204.0     100.0
     205.0      15.8
     206.0       5.5

Assign. Shift(ppm) A 11.8 B 7.46 C 7.41 D 5.778 E *1 4.253 F 3.982 G *2 3.80 J *2 3.77 K *1 3.657

     Hz     ppm     Int.

   2989.28   7.480     33
   2987.63   7.476     78
   2986.35   7.473     72
   2982.32   7.463   1000
   2979.39   7.455    700
   2976.82   7.449    619
   2974.26   7.443     84
   2971.33   7.435     92
   2969.68   7.431    133
   2968.76   7.429    132
   2967.30   7.425     61
   2966.75   7.424     59
   2964.73   7.419    145
   2961.80   7.411    150
   2959.97   7.407    103
   2958.14   7.402    101
   2955.94   7.397    136
   2954.11   7.392     53
   2952.46   7.388     64
   2951.18   7.385     47
   2949.90   7.382     42
   2947.52   7.376     32
   2318.89   5.803    154
   2310.65   5.782    197
   2308.63   5.777    188
   2300.20   5.756    163
   1710.23   4.280    182
   1699.97   4.254    393
   1689.71   4.228    188
   1600.33   4.005    201
   1592.63   3.986    507
   1589.34   3.977     39
   1585.49   3.968    371
   1531.82   3.833     50
   1524.86   3.816     91
   1521.75   3.808    166
   1519.73   3.803     32
   1514.97   3.791    340
   1511.86   3.783     32
   1508.01   3.774    314
   1500.13   3.754    124
   1498.49   3.750     82
   1490.24   3.729     34
   1471.01   3.681    203
   1462.58   3.660    220
   1460.75   3.656    205
   1452.51   3.635    190