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3-Methoxybenzylamine

Product Name 3-Methoxybenzylamine

CAS5071-96-5

MFC8H11NO

MW137.18

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¹HNMR

¹³CNMR

IR1

Mass

MS-NW-5464          
m-methoxybenzylamine
C8H11NO             (Mass of molecular ion:    137)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       2.4
      18.0       2.1
      27.0       2.2
      28.0      18.7
      29.0       3.0
      30.0      41.9
      31.0       1.1
      37.0       1.2
      38.0       3.6
      39.0       9.7
      40.0       1.7
      41.0       3.0
      42.0       2.2
      44.0       3.8
      50.0       5.2
      51.0       8.7
      52.0       3.8
      53.0       2.1
      54.0       1.8
      62.0       2.2
      63.0       7.4
      64.0       5.5
      65.0      12.0
      66.0       7.8
      67.0       5.1
      74.0       1.6
      75.0       1.4
      76.0       2.4
      77.0      22.2
      78.0      12.9
      79.0      10.3
      80.0       1.3
      89.0       2.5
      90.0       2.6
      91.0      12.0
      92.0       5.4
      93.0       9.7
      94.0      19.8
      95.0       4.0
     103.0       1.2
     104.0       6.8
     105.0       7.9
     106.0      45.3
     107.0       7.1
     108.0      12.3
     109.0      24.3
     110.0       2.2
     119.0       5.3
     120.0      12.6
     121.0      21.3
     122.0      17.0
     123.0       1.5
     133.0       1.5
     134.0       2.4
     135.0       1.3
     136.0     100.0
     137.0      73.0
     138.0       7.2
     150.0       2.4
     151.0       1.2
     255.0       1.5

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₁ N O	0.04 ml : 0.5 ml CDCl₃
m-methoxybenzylamine

    Assign.     Shift(ppm)

      A             7.22
      B             6.85
      C             6.84
      D             6.77
      E             3.82
      F             3.790
      G             1.49
     
     400MHZ. : HSP-41-700

     Hz     ppm     Int.

    656.44   7.330     30
    648.63   7.243     87
    640.50   7.152     76
    619.69   6.920     48
    619.13   6.914     57
    618.63   6.908     49
    618.06   6.902     63
    617.44   6.895     44
    615.00   6.867     61
    614.38   6.860     74
    613.50   6.851     60
    612.31   6.837    101
    611.69   6.830    114
    342.31   3.823    234
    339.50   3.791   1000
    133.50   1.491    415

¹H NMR	399.65 MHz
C₈ H₁₁ N O	0.05 ml : 0.5 ml CDCl₃
m-methoxybenzylamine

    Assign.     Shift(ppm)

      A             7.210
      B             6.85
      C             6.84
      D             6.755
      E             3.785
      F             3.752
      G             1.51
     
     90MHZ. : HSP-03-438

     Hz     ppm     Int.

   2890.01   7.232     81
   2881.71   7.211    169
   2874.15   7.192    119
   2742.43   6.863    129
   2742.07   6.862    131
   2734.99   6.844    256
   2733.64   6.841    237
   2704.59   6.768    100
   2702.39   6.762     91
   2697.02   6.749     80
   2695.56   6.745     85
   2693.60   6.740     76
   1512.82   3.786    376
   1499.63   3.753   1000
    604.13   1.512    199

in CDCl3

liquid film

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