-
MassMS-NW-1534 2-pyridinamine C5H6N2 (Mass of molecular ion: 94)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 2.1 27.0 2.1 28.0 12.7 37.5 5.0 38.0 9.0 39.0 20.6 40.0 11.8 41.0 23.8 42.0 2.6 43.0 1.9 47.0 2.7 49.0 1.0 50.0 5.2 51.0 7.3 52.0 4.9 53.0 1.2 54.0 2.2 63.0 1.0 64.0 2.1 65.0 3.1 66.0 12.4 67.0 75.7 68.0 4.7 78.0 1.6 93.0 4.5 94.0 100.0 95.0 6.5
90 MHz in CDCl3
-
1H NMR 89.56 MHz C5 H6 N2 0.041 g : 0.5 ml CDCl3 2-pyridinamine 
Assign. Shift(ppm)
A 8.049 B 7.379 C 6.605 D 6.469 E 4.63 J(A,B)=1.9HZ J(A,C)=5.1HZ J(A,D)=1.0HZ J(B,C)=7.3HZ J(B,D)=8.3HZ J(C,D)=1.0HZ
Hz ppm Int.725.13 8.097 241 724.19 8.087 268 723.19 8.075 296 722.31 8.066 270 719.94 8.039 277 719.13 8.030 301 718.13 8.019 317 717.25 8.009 285 670.63 7.489 395 668.69 7.467 382 663.38 7.408 500 662.38 7.396 523 661.44 7.386 492 660.44 7.375 480 655.19 7.316 589 653.25 7.294 682 598.00 6.678 485 597.00 6.666 586 592.94 6.621 446 591.94 6.610 574 590.81 6.597 471 589.81 6.586 469 585.75 6.541 427 584.75 6.530 492 584.00 6.521 628 583.00 6.510 1000 582.06 6.500 491 575.75 6.429 490 574.81 6.419 816 573.81 6.407 421 414.56 4.629 206
in CDCl3
CCl4 solution
KBr disc
nujol mull
More Suppliers
