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4884-68-8

HYDRASTININE HCL(RG)

Product Name HYDRASTININE HCL(RG)

CAS4884-68-8

MFC11H13NO3.ClH

MW243.689

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  • 4884-68-8_ms_1
    Mass

    MS-NW-6981          
    6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo(4,5-g)isoquinolin-5-ol hydrochloride
    C11H13NO3 HCl       (Mass of molecular ion:    207)
    

       Source Temperature: 230 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          15.0       2.8
          18.0       2.5
          27.0       1.8
          28.0       1.5
          29.0       1.1
          35.0       3.7
          36.0      23.5
          37.0       1.3
          38.0       7.2
          39.0       5.9
          40.0       1.1
          41.0       2.3
          42.0      20.9
          43.0       1.1
          50.0       3.7
          51.0       6.0
          52.0       1.8
          53.0       1.6
          62.0       3.4
          63.0       6.6
          64.0       3.0
          65.0       5.1
          65.5       4.6
          66.0       1.5
          74.0       1.2
          75.0       1.4
          76.0       1.5
          77.0       5.8
          78.0       2.2
          79.0       1.2
          80.5       1.2
          86.0       1.0
          87.0       1.5
          87.5       1.0
          88.0       2.0
          89.0      12.5
          90.0       6.6
          91.0       7.7
          92.0       1.6
          93.5       3.4
          94.0       1.1
          94.5       7.7
          95.0       2.7
         102.0       1.6
         103.0       2.8
         104.0       1.0
         105.0       1.1
         115.0       2.3
         116.0       3.5
         117.0       3.2
         118.0       2.2
         119.0       1.9
         130.0       8.0
         131.0       4.5
         132.0       4.9
         133.0       1.0
         135.0       1.2
         146.0       1.0
         147.0      27.5
         148.0     100.0
         149.0      12.8
         150.0       1.2
         159.0       1.6
         160.0       3.9
         161.0       1.9
         162.0       4.9
         163.0       1.1
         172.0       4.2
         173.0       6.8
         174.0       2.3
         175.0       3.3
         176.0       2.8
         177.0       1.6
         188.0      55.2
         189.0      17.5
         190.0      83.3
         191.0      58.2
         192.0       7.2
    

400 MHz in DMSO-d6 at 50.C

  • 4884-68-8_1hnmr_0

    1H NMR 399.65 MHz
    C11 H12 Cl N O3 0.041 g : 0.5 ml DMSO-d6 at 50 C
    6-methyl-7,8-dihydro-1,3-dioxolo(4,5-g)isoquinolin-5(6H)-one hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.41 B 7.431 C 7.144 D 6.236 E 3.985 F 3.731 G 3.163

         Hz     ppm     Int.
    

       3759.61   9.408    121
       2970.12   7.432    376
       2855.38   7.145    257
       2492.52   6.237   1000
       1601.41   4.008     92
       1593.17   3.987    174
       1584.63   3.966    106
       1491.24   3.732    606
       1275.02   3.191    123
       1266.78   3.170    211
       1258.24   3.149    116
    

D2O

in DMSO-d6

  • 4884-68-8_13cnmr_2

  • 4884-68-8_13cnmr_0

KBr disc

  • 4884-68-8_ir1_2

nujol mull

  • 4884-68-8_ir2_1