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7149-10-2

4-Hydroxy-3-methoxybenzylamine hydrochloride

Product Name 4-Hydroxy-3-methoxybenzylamine hydrochloride

CAS7149-10-2

MFC8H12ClNO2

MW189.64

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  • 7149-10-2_ms
    Mass

    MS2014-05075CW      
    4-aminomethyl-2-methoxyphenol hydrochloride
    C8H11NO2 HCl        (Mass of molecular ion:    153)
    

       Source Temperature: 245 °C
       Sample Temperature:  20 °C
       Direct, 70 eV
    

          15.0       1.5
          27.0       2.3
          28.0       7.2
          29.0       1.7
          30.0      12.5
          35.0       3.3
          36.0      18.4
          37.0       1.1
          38.0       6.2
          39.0       8.4
          40.0       1.5
          41.0       2.4
          42.0       1.0
          43.0       1.1
          50.0       4.2
          51.0       9.6
          52.0       8.5
          53.0       5.8
          54.0       3.7
          55.0       3.8
          62.0       2.3
          63.0       5.0
          64.0       2.8
          65.0      20.0
          66.0       5.7
          67.0       6.1
          68.0       1.0
          76.0       1.2
          77.0       8.6
          78.0       4.1
          79.0       4.2
          80.0      10.0
          81.0      10.0
          82.0       8.6
          83.0       2.5
          90.0       1.6
          91.0       1.8
          92.0       5.0
          93.0      24.8
          94.0      12.0
          95.0       6.2
         105.0       5.6
         106.0       5.4
         107.0      12.7
         108.0       7.2
         109.0      24.3
         110.0      31.4
         111.0       3.8
         118.0       2.0
         119.0       1.1
         120.0       3.9
         121.0       9.4
         122.0      62.9
         123.0       6.5
         124.0       5.3
         125.0      12.9
         126.0       1.0
         134.0       2.2
         135.0       9.5
         136.0      74.5
         137.0      77.2
         138.0      13.8
         139.0       1.2
         150.0       3.0
         151.0       1.1
         152.0      97.8
         153.0     100.0
         154.0       9.0
    

400 MHz in DMSO-d6

  • 7149-10-2_1hnmr

    1H NMR 399.65 MHz
    C8 H11 N O2 0.036 g : 0.5 ml DMSO-d6
    4-aminomethyl-2-methoxyphenol hydrochloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.26 B 8.51 C 7.223 D 6.874 E 6.823 F 3.878 G 3.777

         Hz     ppm     Int.
    

       3702.39   9.265     26
       3399.35   8.506     88
       2887.88   7.227    161
       2886.05   7.222    163
       2753.45   6.890     61
       2751.62   6.886     58
       2745.51   6.870    114
       2743.53   6.865    115
       2729.80   6.831    242
       2721.71   6.811    132
       1552.73   3.886    105
       1547.39   3.872    105
       1509.55   3.778   1000
    

in DMSO-d6

KBr disc

nujol mull