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(-)-EBURNAMONINE

Product Name (-)-EBURNAMONINE

CAS4880-88-0

MFC19H22N2O

MW294.39

¹HNMR

¹³CNMR

IR1

IR2

Mass

MS-IW-0801          
(-)-eburnamonine
C19H22N2O           (Mass of molecular ion:    294)

   Source Temperature: 150 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      41.0       1.0
     115.0       1.1
     118.5       1.1
     147.0       2.9
     167.0       4.7
     168.0       4.7
     169.0       1.4
     180.0       3.7
     181.0       1.5
     193.0       1.0
     194.0       1.3
     196.0       2.6
     208.0       1.4
     209.0       1.8
     210.0       1.1
     222.0       4.0
     223.0       1.7
     224.0      12.8
     225.0       2.8
     235.0       1.4
     236.0       3.7
     237.0      17.5
     238.0       4.5
     248.0       2.0
     251.0       1.9
     252.0       1.0
     263.0       3.7
     264.0       5.4
     265.0      26.7
     266.0       8.1
     267.0       1.1
     293.0      57.5
     294.0     100.0
     295.0      20.5
     296.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₉ H₂₂ N₂ O	0.034 g : 0.5 ml CDCl₃
(-)-eburnamonine

    Assign.     Shift(ppm)

      A             8.364
      B             7.413
      C     *1      7.304
      D     *1      7.275
      E             3.901
      F     *2      3.299
      G     *2      3.193
      J     *3      2.876
      K     *4      2.627
      L     *4      2.570
      M     *5      2.55
      N     *3      2.44
      P     *5      2.38
      Q     *6      2.023
      R     *7      1.741
      S     *6      1.630
      T     *8      1.469
      U     *7      1.368
      V     *8      1.005
      W             0.920
     
     ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   3348.02   8.378    158
   3347.29   8.376    180
   3346.07   8.373    242
   3340.58   8.359    149
   3339.36   8.356    197
   3338.75   8.355    197
   3338.01   8.353    176
   2967.41   7.426    128
   2966.55   7.423    128
   2965.33   7.420    102
   2960.45   7.408    223
   2958.86   7.404    171
   2929.20   7.330     58
   2927.73   7.326     76
   2921.88   7.312    195
   2920.17   7.307    164
   2914.31   7.293    406
   2912.48   7.288    420
   2906.86   7.274    256
   2905.52   7.271    220
   2899.54   7.256     94
   2898.19   7.252     72
   1559.08   3.902    179
   1330.69   3.330     74
   1324.46   3.315     86
   1316.77   3.295    142
   1310.55   3.280    150
   1290.28   3.229     71
   1284.55   3.215     82
   1278.93   3.201     90
   1276.37   3.194     48
   1273.07   3.186     91
   1270.63   3.180     49
   1265.01   3.166     54
   1259.28   3.151     52
   1159.18   2.901     45
   1151.73   2.882     57
   1150.76   2.880     50
   1148.93   2.875     60
   1147.95   2.873     46
   1145.26   2.866     49
   1142.33   2.859     50
   1140.50   2.854     54
   1137.70   2.847     49
   1062.26   2.658    155
   1045.53   2.617    464
   1031.13   2.581    497
   1023.56   2.562     69
   1022.46   2.559     76
   1021.00   2.555     87
   1019.29   2.551     76
   1018.31   2.549     72
   1014.40   2.539    158
    986.08   2.468     70
    983.52   2.461     73
    980.83   2.455     74
    978.27   2.448     72
    969.24   2.426     63
    966.67   2.419     74
    964.23   2.413    100
    961.55   2.406    120
    952.39   2.384     90
    950.44   2.379     80
    949.34   2.376     83
    941.16   2.355     56
    937.87   2.347     52
    821.66   2.056     89
    813.96   2.037    105
    807.25   2.020    138
    806.03   2.017    144
    799.68   2.001    110
    700.56   1.753     65
    696.41   1.743     45
    687.13   1.720     68
    661.50   1.656     80
    654.17   1.637    101
    647.09   1.620     92
    639.77   1.601     72
    594.48   1.488     75
    591.31   1.480     45
    583.74   1.461     50
    580.81   1.454     87
    577.76   1.446     52
    555.79   1.391     57
    552.86   1.384     76
    549.80   1.376     57
    542.36   1.358     50
    539.43   1.350     65
    536.38   1.343     46
    416.63   1.043     57
    412.72   1.033     58
    402.95   1.009    105
    399.17   0.999     99
    389.40   0.975     53
    385.62   0.965     46
    375.12   0.939    484
    367.55   0.920   1000
    359.99   0.901    444

in CDCl3

KBr disc

nujol mull

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