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1-HYDROXYPIPERIDINE

Product Name 1-HYDROXYPIPERIDINE

CAS4801-58-5

MFC5H11NO

MW101.15

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¹HNMR

¹³CNMR

IR1

Mass

MS-NW-5425          
N-hydroxypiperidine
C5H11NO             (Mass of molecular ion:    101)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       5.9
      17.0       8.3
      18.0      36.4
      26.0       7.6
      27.0      29.1
      28.0      46.7
      29.0      23.6
      30.0      14.8
      37.0       1.5
      38.0       3.0
      39.0      22.8
      40.0       5.8
      41.0      53.4
      42.0      46.2
      43.0      11.6
      44.0      12.5
      45.0      23.0
      46.0       7.1
      50.0       3.6
      51.0       5.1
      52.0       6.0
      53.0       7.4
      54.0      23.8
      55.0     100.0
      56.0      33.8
      57.0      17.0
      58.0       1.4
      59.0       6.1
      60.0      12.6
      65.0       1.0
      67.0       4.2
      68.0       7.3
      69.0       2.0
      70.0       5.3
      72.0       2.5
      73.0       6.3
      78.0       1.0
      79.0       4.6
      80.0       4.8
      81.0       3.0
      82.0      20.4
      83.0      48.0
      84.0      55.5
      85.0      21.9
      86.0       1.8
      97.0       1.1
      98.0       1.6
      99.0       3.3
     100.0      63.8
     101.0      33.5
     102.0       2.4

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₅ H₁₁ N O	0.04 ml : 0.5 ml CDCl₃
N-hydroxypiperidine

    Assign.     Shift(ppm)

      A             8.2
      B             3.253
      C             2.449
      D             1.736
      E             1.58
      F             1.56
      G             1.15
     
     J(B,C)=9.8HZ. J(C,D)=2.6HZ.

     Hz     ppm     Int.

   3260.62   8.159     42
   1322.02   3.308     39
   1321.53   3.307     42
   1321.29   3.307     42
   1320.68   3.305     45
   1319.95   3.303     48
   1318.85   3.301     52
   1318.48   3.300     53
   1317.14   3.296     61
   1315.43   3.292     74
   1304.69   3.265    791
   1300.17   3.254    460
   1294.92   3.241    849
   1000.12   2.503     41
    999.15   2.501     46
    998.29   2.498     51
    997.68   2.497     54
    991.09   2.480    507
    988.65   2.474    481
    984.86   2.465    201
    984.25   2.463    200
    978.88   2.450    895
    971.56   2.432    187
    968.38   2.424    524
    965.70   2.417    485
    719.97   1.802     39
    718.99   1.800     42
    717.65   1.796     48
    716.43   1.793     50
    715.09   1.790     58
    714.60   1.789     60
    714.23   1.788     60
    713.87   1.787     61
    710.57   1.778    112
    702.27   1.758    533
    701.90   1.757    531
    699.83   1.752    526
    697.39   1.746    426
    691.65   1.731    564
    688.96   1.724    691
    686.89   1.719    701
    674.93   1.689     56
    673.58   1.686     46
    672.61   1.683     47
    671.39   1.680     43
    670.90   1.679     42
    669.43   1.676     40
    668.09   1.672     42
    667.48   1.671     43
    667.11   1.670     40
    663.57   1.661     40
    661.99   1.657     39
    660.89   1.654     40
    660.28   1.653     39
    659.79   1.651     40
    658.69   1.649     43
    658.33   1.648     46
    657.35   1.645     45
    656.98   1.644     45
    655.40   1.640     55
    654.42   1.638     56
    654.05   1.637     58
    653.69   1.636     58
    651.98   1.632     69
    650.88   1.629     74
    642.21   1.607    391
    639.04   1.599    525
    637.08   1.595    450
    635.74   1.591    471
    627.44   1.570    978
    626.10   1.567   1000
    615.97   1.542    455
    612.30   1.533    562
    609.86   1.526    338
    603.27   1.510    174
    599.73   1.501    231
    595.95   1.492    121
    481.57   1.205     44
    478.76   1.198    112
    474.73   1.188    133
    471.80   1.181     79
    471.31   1.180     77
    470.34   1.177     82
    469.97   1.176     82
    466.55   1.168    245
    462.40   1.158    318
    459.47   1.150    203
    456.42   1.143    103
    454.10   1.137    241
    450.20   1.127    314
    446.17   1.117    134
    442.26   1.107     89
    439.58   1.100     58
    437.99   1.096     50
    437.50   1.095     52
    437.01   1.094     50
    436.40   1.092     52

¹H NMR	89.56 MHz
C₅ H₁₁ N O	0.045 g : 0.5 ml CDCl₃
N-hydroxypiperidine

    Assign.     Shift(ppm)

      A             8.08
      B             3.25
      C             2.44
      D          1.96 to 0.78

     Hz     ppm     Int.

    733.00   8.185     78
    732.19   8.176     89
    731.19   8.165    104
    730.19   8.154    124
    729.88   8.150    136
    724.25   8.087    404
    723.94   8.084    405
    716.81   8.004     97
    297.06   3.317    458
    287.06   3.206    625
    231.06   2.580    234
    230.50   2.574    234
    229.63   2.564    243
    227.75   2.543    304
    225.06   2.513    147
    224.75   2.510    139
    220.75   2.465    449
    220.13   2.458    455
    219.81   2.455    459
    219.31   2.449    455
    217.50   2.429    613
    213.31   2.382    150
    212.81   2.377    152
    212.13   2.369    171
    210.25   2.348    254
    209.94   2.345    259
    209.56   2.340    261
    208.81   2.332    256
    207.06   2.312    318
    165.25   1.846    121
    163.50   1.826    146
    160.63   1.794    254
    157.81   1.763    474
    153.63   1.716    704
    150.56   1.682   1000
    148.31   1.656    875
    147.75   1.650    874
    145.44   1.624    816
    140.44   1.569    499
    138.00   1.541    461
    137.69   1.538    462
    136.63   1.526    446
    136.06   1.520    445
    135.69   1.516    442
    133.00   1.486    515
    132.69   1.482    512
    132.38   1.479    504
    125.06   1.397    162
    124.19   1.387    163
    123.88   1.384    161
    122.00   1.363    199
    121.56   1.358    201
    121.06   1.352    195
    120.56   1.347    198
    118.94   1.329    245
    116.63   1.303    204
    115.13   1.286    170
    114.63   1.280    162
    113.81   1.271    157
    113.44   1.267    158
    112.56   1.257    163
    111.25   1.243    136
    110.44   1.234    130
    108.63   1.213    166
    107.94   1.206    156
    107.38   1.199    146
    106.75   1.192    145
    106.31   1.188    145
    105.06   1.174    176
    103.44   1.155    129
    102.94   1.150    121
    101.56   1.134    143
    100.94   1.128    145
    100.44   1.122    136
     99.94   1.116    137
     98.94   1.105    131
     98.56   1.101    131
     97.94   1.094    132
     96.25   1.075     96
     95.94   1.072     95
     95.63   1.068    100
     94.81   1.059    105
     94.31   1.054    110
     94.00   1.050    109
     92.88   1.038     93
     92.13   1.029     83
     91.56   1.023     86
     90.00   1.005     80
     89.50   1.000     89

in CDCl3

liquid film

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