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2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE

Product Name 2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE

CAS47250-53-3

MFC15H12F6N2

MW334.26

¹³CNMR

Mass

MS-IW-7557          
3,3'-(hexafluoroisopropylidene)dianiline
C15H12F6N2          (Mass of molecular ion:    334)

   Source Temperature: 130 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       2.2
      28.0       1.1
      39.0       1.7
      65.0       2.6
      83.5       3.4
      84.0       1.4
      89.5       1.0
      97.5      10.7
      98.0      14.9
      98.5       2.2
      99.0       1.1
     108.5       1.1
     122.0       2.7
     122.5       2.5
     132.0       3.8
     132.5       5.2
     151.0       1.1
     152.0       1.7
     167.0       6.6
     168.0       1.9
     178.0       1.2
     179.0       1.7
     180.0       5.3
     181.0       1.1
     183.0       1.4
     195.0      15.0
     196.0       8.5
     197.0       1.2
     198.0       4.5
     201.0       1.1
     220.0       1.0
     225.0       3.4
     226.0       1.8
     228.0       1.0
     229.0       2.1
     244.0       3.7
     245.0       3.7
     246.0       1.0
     247.0       1.4
     248.0       8.7
     249.0       8.2
     250.0       1.6
     263.0       3.8
     264.0       8.4
     265.0      31.8
     266.0       5.3
     295.0       2.7
     316.0       2.1
     317.0       4.0
     318.0       3.1
     319.0       1.2
     333.0      19.0
     334.0     100.0
     335.0      16.8
     336.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₅ H₁₂ F₆ N₂	0.040 g : 0.5 ml CDCl₃
3,3'-(hexafluoroisopropylidene)dianiline

    Assign.     Shift(ppm)

      A             7.122
      B             6.814
      C             6.68
      D             6.666
      E             3.61

     Hz     ppm     Int.

   2855.59   7.146    309
   2854.74   7.144    215
   2852.05   7.137     48
   2847.29   7.125    608
   2842.90   7.114     48
   2839.84   7.106    321
   2839.23   7.105    403
   2727.29   6.825    298
   2726.56   6.823    306
   2718.75   6.803    275
   2674.32   6.692    282
   2673.46   6.690    316
   2672.12   6.687    449
   2671.26   6.684    446
   2664.43   6.667    967
   2663.70   6.666   1000
   2653.81   6.641     25
   2652.47   6.637     22
   1442.26   3.609    120

in CDCl3

KBr disc

nujol mull

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2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE(47250-53-3)¹HNMR 2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE(47250-53-3)MS 2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE(47250-53-3)¹³CNMR 2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE(47250-53-3)IR2 2,2-BIS(3-AMINOPHENYL)HEXAFLUOROPROPANE(47250-53-3)IR1

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