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WebSite > CAS DataBase List >  116325-74-7More Spectrum > 2,2-BIS(3-AMINO-4-METHYLPHENYL)HEXAFLUOROPROPANE(116325-74-7)IR1

116325-74-7

2,2-BIS(3-AMINO-4-METHYLPHENYL)HEXAFLUOROPROPANE

Product Name 2,2-BIS(3-AMINO-4-METHYLPHENYL)HEXAFLUOROPROPANE

CAS116325-74-7

MFC17H16F6N2

MW362.31

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  • 116325-74-7_ms_1
    Mass

    MS-IW-1777          
    5,5'-(hexafluoroisopropylidene)bis(o-toluidine)
    C17H16F6N2          (Mass of molecular ion:    362)
    

       Source Temperature: 160 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          77.0       1.1
         104.0       4.3
         104.5       5.1
         111.0       1.0
         112.0       2.0
         129.0       1.2
         131.5       2.3
         138.5       1.7
         139.0       7.5
         139.5       1.2
         146.5       1.0
         166.0       2.7
         173.0       1.0
         173.5       1.8
         180.0       1.3
         181.0       5.0
         207.0       1.9
         208.0       2.7
         209.0       7.2
         210.0       1.3
         211.0       1.1
         223.0       2.3
         224.0       1.3
         258.0       1.2
         263.0       1.9
         275.0       1.8
         276.0       5.4
         277.0       6.5
         278.0      26.9
         279.0       4.6
         291.0       1.5
         292.0       1.8
         293.0      12.1
         294.0       2.2
         323.0       2.2
         331.0       1.3
         332.0       4.8
         333.0       1.0
         344.0       1.1
         345.0       2.6
         346.0       9.9
         347.0       7.3
         348.0       1.2
         361.0       9.9
         362.0     100.0
         363.0      19.3
         364.0       1.8
    

400 MHz in DMSO-d6

  • 116325-74-7_1hnmr_0

    1H NMR 399.65 MHz
    C17 H16 F6 N2 0.032 g : 0.5 ml DMSO-d6
    5,5'-(hexafluoroisopropylidene)bis(o-toluidine)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.956 B 6.616 C 6.465 D 5.01 E 2.046

         Hz     ppm     Int.
    

       2783.94   6.966    172
       2775.51   6.945    185
       2644.04   6.616    189
       2587.65   6.475     98
       2579.83   6.456     92
       2001.10   5.008    377
        817.87   2.047   1000
        808.35   2.023     22
        807.37   2.021     22
        807.13   2.020     22
    

in DMSO-d6

  • 116325-74-7_13cnmr_0

KBr disc

  • 116325-74-7_ir1_2

nujol mull

  • 116325-74-7_ir2_1