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MS-IW-9528 4-chloro-2-fluorotoluene C7H6ClF (Mass of molecular ion: 144)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 1.4 31.0 1.5 38.0 1.0 39.0 2.5 43.0 1.2 44.0 4.9 50.0 2.4 51.0 1.8 53.5 1.0 54.0 4.0 57.0 5.4 61.0 1.9 62.0 3.6 63.0 4.2 72.0 1.5 73.0 1.7 74.0 1.2 75.0 1.1 81.0 3.7 83.0 8.9 89.0 2.0 91.0 1.0 93.0 1.0 107.0 10.0 108.0 4.0 109.0 100.0 110.0 7.8 117.0 2.5 143.0 20.0 144.0 34.9 145.0 8.9 146.0 11.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 Cl F 0.05 ml : 0.5 ml CDCl3 4-chloro-2-fluorotoluene Assign. Shift(ppm)
A 7.06 B 6.99 C 2.207
Hz ppm Int.
2829.10 7.079 136 2821.17 7.060 275 2813.23 7.040 170 2812.50 7.038 189 2799.56 7.006 207 2797.61 7.001 429 2796.14 6.997 351 2789.92 6.981 228 2788.33 6.977 528 2786.38 6.973 144 883.42 2.211 1000
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