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MS-KW-0549 2-fluoro-m-xylene C8H9F (Mass of molecular ion: 124)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.9 39.0 3.4 50.0 2.3 51.0 7.0 52.0 1.1 57.0 3.3 60.0 1.5 61.0 3.3 62.0 1.3 63.0 2.8 70.0 1.3 74.0 1.1 75.0 2.6 77.0 8.3 78.0 1.5 81.0 1.5 83.0 4.8 95.0 2.1 96.0 4.0 97.0 2.8 101.0 3.8 102.0 1.5 103.0 5.6 107.0 1.5 109.0 100.0 110.0 7.5 121.0 2.6 122.0 2.7 123.0 31.3 124.0 56.3 125.0 4.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C8H9F 0.05 ml : 0.5 ml CDCl3 2-fluoro-1,3-dimethylbenzene Assign. Shift(ppm)
A 6.960 B 6.883 C 2.238
Hz ppm Int.
2790.90 6.982 119 2790.53 6.981 116 2783.45 6.963 264 2776.25 6.945 184 2775.88 6.944 182 2757.45 6.898 184 2750.74 6.881 115 2749.15 6.877 120 2742.56 6.861 74 895.63 2.241 1000 893.32 2.235 933
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