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tert-Butyl carbamate

Product Name tert-Butyl carbamate

CAS4248-19-5

MFC5H11NO2

MW117.15

¹³CNMR

Mass

MS2014-05021CW      
tert-butyl carbamate
C5H11NO2            (Mass of molecular ion:    117)

   Source Temperature: 250 °C
   Sample Temperature: 200 °C
   Reservoir, 70 eV

      15.0       2.4
      17.0       1.1
      26.0       1.3
      27.0       8.1
      28.0      11.6
      29.0      21.0
      31.0      13.7
      32.0      10.1
      38.0       2.0
      39.0      18.3
      40.0       3.8
      41.0      65.5
      42.0       2.6
      43.0      11.3
      44.0      17.4
      45.0       1.0
      50.0       2.0
      51.0       2.2
      53.0       2.4
      55.0       9.4
      56.0      36.9
      57.0      65.0
      58.0       3.4
      59.0     100.0
      60.0       3.3
      62.0      29.1
     102.0       2.9

parameter in CDCl3

¹H NMR	300 MHz
C₅ H₁₁ N O₂	0.050 g : 0.5 ml CDCl₃
tert-butyl carbamate

    Parameter     ppm  Hz

      D(A)         4.70
     
      D(B)         1.449

     Hz     ppm     Int.

   1410.00   4.700     36
    434.71   1.449   1000

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

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