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MS-NW-7080 N-benzylethylenediamine C9H14N2 (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 3.4 28.0 3.6 30.0 11.5 39.0 3.2 41.0 1.8 42.0 1.9 43.0 1.2 44.0 2.8 50.0 1.1 51.0 2.7 63.0 1.9 65.0 8.7 77.0 2.0 79.0 1.5 89.0 2.0 90.0 1.4 91.0 100.0 92.0 9.1 104.0 1.2 106.0 5.9 107.0 1.7 118.0 2.7 119.0 1.7 120.0 43.9 121.0 5.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H14 N2 0.04 ml : 0.5 ml CDCl3 N-benzylethylenediamine Assign. Shift(ppm)
A 7.30 B 3.789 C 2.74 D 1.46
Hz ppm Int.
656.25 7.328 183 653.69 7.299 888 651.25 7.272 251 650.63 7.265 182 339.38 3.790 559 255.63 2.855 62 250.50 2.798 125 249.94 2.791 125 249.13 2.782 82 247.06 2.759 212 246.44 2.752 247 244.00 2.725 264 243.38 2.718 242 241.38 2.696 93 240.50 2.686 138 239.63 2.676 137 238.69 2.666 65 234.81 2.622 71 130.50 1.458 1000
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