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41317-15-1More Spectrum > Methoxymethyldiphenylamine(41317-15-1)13CNMR
Methoxymethyldiphenylamine
Product Name Methoxymethyldiphenylamine
CAS41317-15-1
MFC14H15NO
MW213.27
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MS-KW-0183 4-methoxy-2-methyldiphenylamine C14H15NO (Mass of molecular ion: 213)
Source Temperature: 140 °C Sample Temperature: 110 °C Direct, 75 eV
39.0 1.8 51.0 3.8 52.0 1.4 63.0 1.0 65.0 2.2 76.0 1.1 77.0 6.9 78.0 1.7 83.5 3.1 90.0 2.1 90.5 2.0 91.0 1.2 92.0 1.1 99.0 2.5 103.0 1.0 105.5 1.4 106.0 1.2 106.5 7.0 107.0 1.2 115.0 1.1 128.0 2.7 130.0 2.1 143.0 1.2 154.0 3.4 155.0 2.7 167.0 3.6 168.0 3.6 169.0 1.6 170.0 2.1 180.0 4.8 181.0 2.6 182.0 1.2 183.0 1.1 196.0 1.9 197.0 1.4 198.0 100.0 199.0 14.8 200.0 1.3 210.0 1.5 212.0 2.2 213.0 92.9 214.0 14.8 215.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H15 N O 0.038 g : 0.5 ml CDCl3 4-methoxy-2-methyldiphenylamine Assign. Shift(ppm)
A 7.166 B 7.125 C 6.79 D 6.77 E 6.72 F 6.70 G 5.16 J 3.778 K 2.202
Hz ppm Int.
2872.31 7.188 124 2871.46 7.185 50 2870.24 7.182 44 2864.99 7.169 162 2863.77 7.166 157 2858.40 7.153 52 2857.18 7.150 59 2856.32 7.148 147 2852.05 7.137 123 2843.38 7.115 132 2715.58 6.795 85 2712.89 6.789 125 2711.91 6.786 130 2710.82 6.783 53 2705.57 6.770 52 2704.47 6.768 115 2703.49 6.765 58 2698.24 6.752 32 2697.14 6.749 58 2696.04 6.747 35 2690.06 6.732 64 2689.58 6.730 65 2687.01 6.724 53 2686.65 6.723 53 2681.40 6.710 89 2680.30 6.707 179 2679.08 6.704 205 2678.34 6.702 137 2677.12 6.699 63 2673.58 6.690 55 2672.61 6.688 89 2671.63 6.685 169 2670.53 6.683 145 2064.33 5.166 34 1509.89 3.779 1000 880.00 2.202 535
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