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MS-NW-6687 4'-morpholinoacetophenone C12H15NO2 (Mass of molecular ion: 205)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 2.6 18.0 1.0 27.0 3.3 28.0 3.6 29.0 1.2 39.0 2.4 41.0 1.1 42.0 4.1 43.0 11.4 50.0 3.5 51.0 6.4 52.0 1.5 57.0 2.9 58.5 1.7 63.0 3.2 64.0 1.0 65.0 2.6 65.5 3.0 66.0 1.4 72.5 1.0 74.0 1.2 75.0 1.9 76.0 4.9 77.0 14.6 78.0 5.7 79.0 1.3 89.0 2.1 90.0 2.9 91.0 6.1 92.0 1.0 102.0 1.4 103.0 2.3 104.0 8.8 105.0 3.1 106.0 1.1 117.0 2.1 118.0 2.6 119.0 2.1 130.0 1.1 132.0 91.7 133.0 9.9 146.0 2.8 147.0 46.2 148.0 5.8 174.0 3.4 175.0 2.4 176.0 2.1 190.0 40.4 191.0 5.2 204.0 5.9 205.0 100.0 206.0 13.6 207.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C12 H15 N O2 0.038 g : 0.5 ml CDCl3 4'-morpholinoacetophenone Assign. Shift(ppm)
A 7.883 B 6.866 C 3.843 D 3.300 E 2.519
Hz ppm Int.
710.94 7.939 145 708.81 7.915 38 704.00 7.861 40 701.81 7.837 175 618.94 6.911 132 616.81 6.888 34 611.94 6.833 30 609.81 6.809 107 349.88 3.907 102 345.19 3.855 135 343.19 3.832 64 340.13 3.798 165 300.13 3.352 153 296.88 3.315 62 295.00 3.294 126 290.25 3.241 101 225.63 2.520 1000
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