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MS-NW-6682 4-morpholinobenzophenone C17H17NO2 (Mass of molecular ion: 267)
Source Temperature: 220 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 3.6 28.0 2.6 39.0 2.9 42.0 4.4 50.0 3.1 51.0 9.2 57.0 3.1 63.0 1.4 65.0 2.2 65.5 1.1 75.0 2.8 76.0 8.1 77.0 25.2 78.0 11.6 89.0 1.1 90.0 5.5 90.5 4.3 91.0 2.4 102.0 1.2 103.0 2.1 104.0 12.0 104.5 1.1 105.0 18.9 106.0 3.9 117.0 1.5 118.0 1.0 119.5 2.4 132.0 100.0 133.0 5.5 151.0 1.0 152.0 3.8 153.0 2.1 167.0 1.3 181.0 5.4 190.0 2.6 209.0 9.0 210.0 1.6 266.0 1.2 267.0 10.4 268.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C17 H17 N O2 0.044 g : 0.5 ml CDCl3 4-morpholinobenzophenone Assign. Shift(ppm)
A 7.78 B 7.74 C 7.52 D 7.48 E 6.883 F 3.843 G 3.310
Hz ppm Int.
705.63 7.879 40 702.88 7.849 457 700.75 7.825 139 697.81 7.792 203 695.81 7.770 323 693.75 7.747 629 691.13 7.717 237 689.44 7.699 102 688.19 7.685 377 686.56 7.666 76 684.44 7.643 40 681.94 7.615 46 677.38 7.564 78 676.19 7.551 96 675.69 7.545 91 674.56 7.532 79 673.06 7.516 253 672.19 7.506 422 670.75 7.490 363 669.81 7.479 200 669.19 7.472 148 668.19 7.461 123 666.56 7.443 124 665.75 7.434 153 664.88 7.424 191 661.19 7.383 37 659.75 7.367 67 623.38 6.961 42 620.63 6.930 426 618.44 6.906 119 613.63 6.852 92 611.50 6.828 343 608.75 6.798 37 349.75 3.906 613 345.13 3.854 830 343.06 3.831 431 340.00 3.797 1000 336.25 3.755 36 300.81 3.359 948 297.63 3.324 415 295.69 3.302 801 291.00 3.250 609
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