4-METHOXY-3-NITROBENZOTRIFLUORIDE

Mass

MS-NW-8792          
2-nitro-4-(trifluoromethyl)anisole
C8H6F3NO3           (Mass of molecular ion:    221)

   Source Temperature: 270 °C
   Sample Temperature: 120 °C
   Reservoir, 75 eV

      15.0       2.7
      28.0       3.3
      29.0       2.0
      30.0       8.8
      31.0       7.7
      37.0       1.5
      38.0       2.4
      39.0       1.9
      50.0       7.9
      51.0       6.2
      53.0       4.2
      56.0       1.0
      57.0       4.6
      61.0       2.2
      62.0       7.3
      63.0      32.7
      64.0       2.5
      65.0       1.2
      68.0       1.2
      69.0       6.4
      70.0       1.5
      74.0       5.1
      75.0      16.3
      76.0       4.9
      77.0       3.7
      78.0       2.4
      79.0       1.8
      81.0       6.5
      82.0       3.0
      83.0       3.3
      87.0       1.5
      88.0       1.8
      93.0       1.7
      94.0       3.8
      95.0      18.4
      96.0       3.3
      99.0       2.5
     100.0       1.4
     101.0       2.9
     106.0       1.9
     107.0       3.6
     110.0       3.4
     112.0       3.7
     113.0      10.5
     114.0       2.0
     115.0       3.4
     119.0       3.2
     120.0       6.7
     123.0       1.4
     125.0      12.1
     126.0      23.0
     127.0      15.6
     128.0       1.7
     129.0       1.4
     131.0       1.5
     132.0      33.7
     133.0       9.9
     141.0      13.5
     142.0       1.7
     143.0       8.6
     144.0       4.2
     145.0      84.7
     146.0      28.1
     147.0       9.5
     148.0       6.7
     149.0       1.2
     159.0       1.2
     160.0      65.3
     161.0      46.8
     162.0       6.0
     163.0      22.3
     164.0       2.8
     174.0     100.0
     175.0       9.7
     176.0       1.7
     177.0       1.1
     188.0       1.1
     191.0      73.6
     192.0      10.7
     202.0      19.2
     203.0       1.8
     205.0       1.1
     207.0       3.4
     221.0      62.8
     222.0       6.5

Assign. Shift(ppm) A 8.113 B 7.81 C 7.250 D 4.045

     Hz     ppm     Int.

    727.81   8.127     98
    725.63   8.103    106
    705.81   7.881     54
    705.25   7.875     52
    704.19   7.863     37
    703.50   7.856     44
    703.00   7.850     39
    697.00   7.783     71
    696.44   7.777     68
    695.50   7.766     48
    694.69   7.757     61
    694.06   7.750     52
    652.50   7.286    141
    643.75   7.188     73
    368.06   4.110     24
    362.31   4.046   1000