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MS-NW-0793 alpha,alpha,alpha-trifluoro-3-nitrotoluene C7H4F3NO2 (Mass of molecular ion: 191)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 2.7 30.0 11.6 31.0 1.0 37.0 1.4 38.0 1.9 39.0 1.8 50.0 9.8 51.0 3.2 57.0 3.4 61.0 1.0 62.0 1.5 63.0 2.7 69.0 4.7 73.0 1.1 74.0 6.0 75.0 15.5 76.0 3.9 81.0 1.5 83.0 2.8 94.0 1.6 95.0 21.0 96.0 1.3 99.0 2.8 113.0 3.3 119.0 2.6 125.0 11.5 126.0 5.7 133.0 10.2 143.0 1.3 144.0 1.3 145.0 100.0 146.0 7.6 161.0 6.0 172.0 10.8 175.0 1.4 191.0 42.9 192.0 3.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H4 F3 N O2 0.04 ml : 0.5 ml CDCl3 alpha,alpha,alpha-trifluoro-3-nitrotoluene Assign. Shift(ppm)
A 8.50 B 8.48 C 7.98 D 7.763
Hz ppm Int.
764.25 8.534 193 763.50 8.526 335 762.19 8.511 921 762.06 8.509 921 761.31 8.501 1000 760.69 8.494 925 754.50 8.425 287 754.06 8.420 325 753.19 8.410 369 752.75 8.405 416 750.88 8.385 246 750.56 8.381 229 722.44 8.067 61 721.81 8.060 139 721.19 8.053 187 720.25 8.043 255 719.75 8.037 263 718.81 8.027 205 718.13 8.019 166 714.00 7.973 316 713.38 7.966 418 712.69 7.958 475 711.75 7.948 515 711.00 7.939 384 710.31 7.932 303 708.69 7.914 47 703.88 7.860 50 702.00 7.839 341 701.19 7.830 471 700.38 7.821 362 694.25 7.752 355 693.44 7.743 556 692.69 7.735 420 690.94 7.715 55 687.44 7.676 45 686.56 7.666 120 685.69 7.657 183 684.88 7.648 153 684.19 7.640 64
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