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4-Bromo-2-fluoroaniline

Product Name 4-Bromo-2-fluoroaniline

CAS367-24-8

MFC6H5BrFN

MW190.01

Mass

MS-NW-9393          
4-bromo-2-fluoroaniline
C6H5BrFN            (Mass of molecular ion:    189)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       4.1
      28.0       4.2
      31.0       4.5
      33.0       1.2
      37.0       2.6
      38.0       3.5
      39.0       4.8
      40.0       1.1
      41.0       2.9
      44.5       1.9
      49.0       1.1
      50.0       3.3
      51.0       2.2
      52.0       5.1
      54.5       8.2
      55.0       3.4
      56.0       2.9
      57.0      13.8
      59.0       1.5
      61.0       4.0
      62.0       5.2
      63.0      17.5
      64.0       3.0
      65.0       2.0
      68.0       1.2
      74.0       1.3
      80.0       1.9
      81.0       7.4
      82.0       7.3
      83.0      39.1
      84.0       5.0
      89.0       2.0
      90.0      28.1
      91.0       2.5
      94.5       5.3
      95.5       5.2
     108.0       1.7
     109.0       5.2
     110.0      48.4
     111.0       3.7
     161.0       4.3
     163.0       4.2
     169.0       1.5
     171.0       1.5
     188.0       1.1
     189.0     100.0
     190.0       8.1
     191.0      97.1
     192.0       6.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₅ Br F N	0.077 g : 0.5 ml CDCl₃
4-bromo-2-fluoroaniline

    Assign.     Shift(ppm)

      A             7.123
      B             7.031
      C             6.628
      D             3.72

     Hz     ppm     Int.

   2853.03   7.139    906
   2850.95   7.134    990
   2848.27   7.127     47
   2842.53   7.113    904
   2840.33   7.108   1000
   2837.77   7.101     44
   2816.04   7.047    591
   2814.94   7.044    608
   2813.96   7.042    542
   2812.74   7.039    504
   2807.62   7.026    641
   2806.40   7.023    661
   2805.54   7.020    600
   2804.32   7.017    560
   2657.47   6.650    879
   2649.05   6.629    943
   2648.07   6.626    965
   2639.65   6.605    792
   1484.99   3.716    186

KBr disc

nujol mull

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