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MassMS-NW-1127 o-fluorophenol C6H5FO (Mass of molecular ion: 112)
Source Temperature: 240 °C Sample Temperature: 170 °C Reservoir, 75 eV
18.0 1.0 27.0 1.0 28.0 2.5 29.0 1.2 31.0 3.8 37.0 2.2 38.0 4.5 39.0 4.6 45.0 1.0 50.0 2.5 51.0 1.6 53.0 2.8 55.0 1.1 56.0 5.1 57.0 11.5 58.0 1.6 61.0 1.6 62.0 2.5 63.0 18.4 64.0 53.7 65.0 3.6 68.0 1.0 73.0 2.1 75.0 1.0 81.0 2.2 82.0 1.2 83.0 12.0 84.0 2.6 92.0 19.8 93.0 1.5 111.0 1.2 112.0 100.0 113.0 6.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 F O 0.05 ml : 0.5 ml CDCl3 o-fluorophenol 
Assign. Shift(ppm)
A 7.02 B 7.00 C 6.97 D 6.810 E 5.88
Hz ppm Int.2822.51 7.063 34 2818.36 7.053 275 2817.99 7.052 275 2816.89 7.049 324 2810.18 7.032 361 2808.72 7.028 428 2807.50 7.025 337 2806.52 7.023 542 2805.66 7.021 384 2804.81 7.019 299 2798.71 7.003 677 2798.34 7.002 635 2797.49 7.000 541 2796.63 6.998 661 2793.95 6.991 389 2792.48 6.988 1000 2791.50 6.985 931 2788.94 6.979 562 2788.45 6.978 525 2786.87 6.974 797 2785.40 6.970 749 2778.81 6.954 236 2777.34 6.950 228 2732.42 6.838 278 2730.35 6.832 284 2727.54 6.825 289 2725.22 6.820 251 2724.12 6.817 435 2723.27 6.815 327 2722.17 6.812 373 2719.48 6.805 259 2718.38 6.802 269 2717.04 6.799 247 2716.19 6.797 264 2715.09 6.794 238 2713.38 6.790 208 2710.21 6.782 191 2350.34 5.881 594 2346.68 5.872 597
in CDCl3
liquid film
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