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MassMS-IW-1081 9,10-dibenzylanthracene C28H22 (Mass of molecular ion: 358)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
91.0 1.5 103.0 1.4 126.0 1.4 131.5 1.0 132.5 3.9 133.0 1.0 138.0 1.0 139.0 3.5 139.5 1.1 140.0 4.3 140.5 1.0 163.0 1.6 165.0 1.5 169.5 1.0 178.0 1.9 179.0 1.7 189.0 1.6 202.0 4.0 203.0 4.7 204.0 1.1 239.0 1.5 252.0 12.4 253.0 3.6 263.0 2.6 264.0 1.3 265.0 22.7 266.0 11.1 267.0 42.0 268.0 10.5 269.0 1.5 276.0 2.0 277.0 2.0 278.0 2.5 279.0 5.3 280.0 3.1 281.0 9.6 282.0 2.2 356.0 1.0 357.0 1.4 358.0 100.0 359.0 30.9 360.0 4.7
400 MHz in CDCl3
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1H NMR 399.65 MHz C28 H22 saturated in CDCl3 9,10-dibenzylanthracene 
Assign. Shift(ppm)
A 8.262 B 7.427 C 7.206 D 7.15 to 7.12 E 5.037
Hz ppm Int.3310.91 8.285 63 3309.81 8.282 83 3307.25 8.276 569 3303.96 8.268 441 3300.29 8.258 439 3297.00 8.250 612 3294.43 8.244 89 3293.33 8.241 71 2977.05 7.450 76 2975.95 7.447 99 2973.39 7.440 649 2970.09 7.432 482 2966.43 7.423 489 2963.13 7.415 620 2960.57 7.408 87 2959.47 7.406 69 2890.87 7.234 37 2889.40 7.230 113 2888.18 7.227 189 2886.35 7.223 123 2884.16 7.217 301 2881.96 7.212 251 2880.74 7.209 411 2879.76 7.206 340 2873.78 7.191 608 2860.23 7.157 483 2858.64 7.153 643 2855.83 7.146 264 2853.39 7.140 344 2850.83 7.134 352 2846.68 7.123 116 2013.31 5.038 1000
in CDCl3
KBr disc
nujol mull
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