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MS-NW-2462 9-methylanthracene C15H12 (Mass of molecular ion: 192)
Source Temperature: 290 °C Sample Temperature: 170 °C Reservoir, 75 eV
63.0 1.6 69.5 1.3 75.0 1.0 81.5 2.1 82.0 1.9 82.5 5.3 83.0 1.6 88.0 1.3 89.0 1.1 93.5 1.5 94.0 2.0 94.5 6.5 95.0 3.7 95.5 3.0 96.0 6.3 96.5 1.1 139.0 1.2 151.0 1.1 152.0 1.7 163.0 2.1 164.0 1.4 165.0 6.8 166.0 1.0 176.0 2.2 178.0 6.2 179.0 1.1 187.0 1.8 188.0 1.7 189.0 17.7 190.0 7.9 191.0 52.5 192.0 100.0 193.0 15.5 194.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C15 H12 18.3 mg : 0.5 ml CDCl3 9-methylanthracene Assign. Shift(ppm)
A 8.314 B 8.268 C 7.981 D 7.49 E 7.45 F 3.076
Hz ppm Int.
3322.88 8.315 186 3310.06 8.283 128 3309.20 8.281 204 3308.23 8.278 216 3307.01 8.275 115 3301.51 8.262 126 3300.42 8.259 242 3299.32 8.256 229 3298.22 8.253 117 3194.70 7.994 194 3193.97 7.992 201 3193.24 7.991 163 3186.52 7.974 234 3185.91 7.972 199 3184.94 7.970 201 3002.81 7.514 100 3001.22 7.510 115 2996.22 7.498 205 2994.75 7.494 209 2992.55 7.488 104 2987.67 7.476 235 2985.96 7.472 200 2983.76 7.466 207 2982.30 7.463 235 2980.59 7.459 42 2977.29 7.450 120 2975.59 7.446 226 2974.24 7.443 200 2970.83 7.434 32 2968.99 7.429 107 2967.77 7.426 94 1229.74 3.078 1000 1229.00 3.076 904
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