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2,6-DIPHENYLPYRIDINE

Product Name 2,6-DIPHENYLPYRIDINE

CAS3558-69-8

MFC17H13N

MW231.29

¹³CNMR

Mass

MS-NW-7799          
2,6-diphenylpyridine
C17H13N             (Mass of molecular ion:    231)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      27.0       1.5
      39.0       2.8
      50.0       3.5
      51.0       7.1
      52.0       2.2
      62.0       1.3
      63.0       3.2
      74.0       2.2
      75.0       3.4
      76.0       4.7
      77.0       7.8
      78.0       1.4
      87.0       1.0
      88.0       1.1
      89.0       2.0
     101.0       3.4
     102.0      11.5
     103.0       1.8
     104.0       1.0
     114.0       2.8
     114.5       1.4
     115.0       2.5
     115.5       3.3
     126.0       3.1
     127.0       6.5
     128.0       3.5
     152.0       2.0
     153.0       1.9
     154.0       3.6
     202.0       5.9
     203.0       2.8
     204.0       2.9
     228.0       4.3
     229.0       2.7
     230.0      46.1
     231.0     100.0
     232.0      17.9
     233.0       1.7

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₇ H₁₃ N	0.019 g : 0.5 ml CDCl₃
2,6-diphenylpyridine

    Assign.     Shift(ppm)

      A             8.14
      B             7.79
      C             7.67
      D             7.49
      E             7.40

     Hz     ppm     Int.

    734.75   8.205    425
    732.00   8.174    232
    731.69   8.170    232
    729.94   8.151    232
    726.69   8.115    536
    724.94   8.095    551
    697.25   7.786    200
    692.63   7.734    440
    689.69   7.701    665
    689.19   7.696    713
    684.56   7.644    290
    679.94   7.593    133
    676.69   7.556    167
    675.06   7.538    101
    672.00   7.504    427
    669.56   7.477    361
    666.63   7.444    820
    664.88   7.424   1000

¹H NMR	399.65 MHz
C₁₇ H₁₃ N	18.8 mg : 0.5 ml CDCl₃
2,6-diphenylpyridine

    Assign.     Shift(ppm)

      A             8.153
      B             7.797
      C             7.684
      D             7.496
      E             7.431

     Hz     ppm     Int.

   3263.43   8.166    675
   3261.96   8.163    943
   3259.89   8.157    245
   3256.47   8.149    406
   3255.00   8.145    874
   3253.66   8.142    670
   3251.59   8.137    152
   3124.88   7.820    194
   3117.80   7.802    240
   3116.46   7.798    279
   3109.25   7.780    354
   3077.76   7.702     35
   3077.03   7.700     33
   3074.34   7.693    901
   3070.19   7.683     37
   3069.09   7.680     34
   3066.77   7.674    561
   3066.04   7.672    467
   3064.33   7.668     55
   3063.96   7.667     56
   3007.45   7.526     44
   3004.52   7.518    269
   3003.42   7.516    436
   3001.71   7.511    176
   2996.34   7.498   1000
   2994.87   7.494    502
   2990.11   7.482    327
   2988.77   7.479    656
   2986.57   7.473    154
   2978.39   7.453     47
   2976.07   7.447    259
   2974.73   7.444    460
   2973.39   7.440    254
   2969.73   7.431    167
   2967.41   7.426    475
   2964.97   7.419    136
   2961.43   7.411    113
   2960.21   7.408    173
   2958.86   7.404     92

in CDCl3

KBr disc

nujol mull

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