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MassMS-NW-7799 2,6-diphenylpyridine C17H13N (Mass of molecular ion: 231)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 1.5 39.0 2.8 50.0 3.5 51.0 7.1 52.0 2.2 62.0 1.3 63.0 3.2 74.0 2.2 75.0 3.4 76.0 4.7 77.0 7.8 78.0 1.4 87.0 1.0 88.0 1.1 89.0 2.0 101.0 3.4 102.0 11.5 103.0 1.8 104.0 1.0 114.0 2.8 114.5 1.4 115.0 2.5 115.5 3.3 126.0 3.1 127.0 6.5 128.0 3.5 152.0 2.0 153.0 1.9 154.0 3.6 202.0 5.9 203.0 2.8 204.0 2.9 228.0 4.3 229.0 2.7 230.0 46.1 231.0 100.0 232.0 17.9 233.0 1.7
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C17 H13 N 0.019 g : 0.5 ml CDCl3 2,6-diphenylpyridine 
Assign. Shift(ppm)
A 8.14 B 7.79 C 7.67 D 7.49 E 7.40
Hz ppm Int.734.75 8.205 425 732.00 8.174 232 731.69 8.170 232 729.94 8.151 232 726.69 8.115 536 724.94 8.095 551 697.25 7.786 200 692.63 7.734 440 689.69 7.701 665 689.19 7.696 713 684.56 7.644 290 679.94 7.593 133 676.69 7.556 167 675.06 7.538 101 672.00 7.504 427 669.56 7.477 361 666.63 7.444 820 664.88 7.424 1000
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1H NMR 399.65 MHz C17 H13 N 18.8 mg : 0.5 ml CDCl3 2,6-diphenylpyridine Assign. Shift(ppm)
A 8.153 B 7.797 C 7.684 D 7.496 E 7.431
Hz ppm Int.3263.43 8.166 675 3261.96 8.163 943 3259.89 8.157 245 3256.47 8.149 406 3255.00 8.145 874 3253.66 8.142 670 3251.59 8.137 152 3124.88 7.820 194 3117.80 7.802 240 3116.46 7.798 279 3109.25 7.780 354 3077.76 7.702 35 3077.03 7.700 33 3074.34 7.693 901 3070.19 7.683 37 3069.09 7.680 34 3066.77 7.674 561 3066.04 7.672 467 3064.33 7.668 55 3063.96 7.667 56 3007.45 7.526 44 3004.52 7.518 269 3003.42 7.516 436 3001.71 7.511 176 2996.34 7.498 1000 2994.87 7.494 502 2990.11 7.482 327 2988.77 7.479 656 2986.57 7.473 154 2978.39 7.453 47 2976.07 7.447 259 2974.73 7.444 460 2973.39 7.440 254 2969.73 7.431 167 2967.41 7.426 475 2964.97 7.419 136 2961.43 7.411 113 2960.21 7.408 173 2958.86 7.404 92
in CDCl3
KBr disc
nujol mull
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