METHYL 5-CHLORO-2-METHOXYBENZOATE

Mass

MS-IW-8998          
methyl 5-chloro-2-methoxybenzoate
C9H9ClO3            (Mass of molecular ion:    200)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       4.1
      28.0       1.5
      29.0       1.7
      37.0       1.4
      38.0       1.3
      39.0       1.2
      45.0       2.9
      50.0       4.1
      51.0       3.4
      53.0       2.2
      59.0       3.3
      61.0       2.7
      62.0       5.0
      63.0      17.7
      64.0       1.3
      65.0       1.6
      72.0       1.1
      73.0       2.1
      74.0       4.2
      75.0      11.9
      76.0       3.7
      77.0       9.7
      78.0       1.5
      79.0       1.2
      91.0       2.2
      93.0       1.0
      97.0       1.2
      98.0       6.2
      99.0       2.0
     100.0       2.4
     110.0       2.2
     111.0      21.2
     112.0       2.7
     113.0       9.7
     114.0       1.1
     115.0       1.0
     126.0      20.1
     127.0       3.1
     128.0       6.6
     129.0       2.3
     133.0       1.2
     135.0       1.3
     139.0      13.2
     140.0       3.8
     141.0       7.4
     142.0       1.6
     143.0       1.1
     154.0       7.8
     155.0       3.2
     156.0       2.8
     157.0       1.5
     167.0      42.8
     168.0       7.8
     169.0     100.0
     170.0      10.3
     171.0      37.3
     172.0       3.4
     173.0       3.2
     183.0       1.2
     185.0       2.3
     200.0      41.5
     201.0       4.5
     202.0      13.6
     203.0       1.5

Assign. Shift(ppm) A 7.753 B 7.394 C 6.904 D *1 3.883 E *1 3.875

     Hz     ppm     Int.

   3100.71   7.759    222
   3097.90   7.752    236
   2961.18   7.410    143
   2958.37   7.403    130
   2952.27   7.388    155
   2949.46   7.381    143
   2763.67   6.916    178
   2754.76   6.893    167
   1551.88   3.884   1000
   1548.71   3.876    785