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MS-NW-3409 methyl o-methoxybenzoate C9H10O3 (Mass of molecular ion: 166)
Source Temperature: 300 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 3.8 29.0 2.3 37.0 1.5 38.0 4.1 39.0 3.4 45.0 1.7 50.0 6.4 51.0 8.5 52.0 1.6 53.0 2.3 59.0 1.5 61.0 1.3 62.0 3.1 63.0 12.0 64.0 10.7 65.0 2.5 74.0 2.6 75.0 2.0 76.0 5.2 77.0 42.4 78.0 4.6 79.0 4.5 91.0 2.8 92.0 22.9 93.0 2.5 95.0 1.4 104.0 1.6 105.0 16.2 106.0 2.6 107.0 2.6 120.0 4.4 121.0 2.5 133.0 34.3 134.0 7.2 135.0 100.0 136.0 9.0 137.0 8.4 149.0 1.1 151.0 2.2 166.0 30.7 167.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 O3 0.04 ml : 0.5 ml CDCl3 methyl o-methoxybenzoate Assign. Shift(ppm)
A 7.78 B 7.44 C 6.97 D 6.97 E *1 3.89 F *1 3.88
Hz ppm Int.
702.25 7.842 59 700.38 7.821 52 700.00 7.816 43 694.25 7.752 70 692.75 7.736 60 692.31 7.731 49 669.00 7.470 38 668.44 7.464 36 666.19 7.439 31 660.88 7.380 44 659.00 7.359 38 630.31 7.038 61 628.13 7.014 59 627.00 7.001 52 623.88 6.967 53 623.38 6.961 60 622.75 6.954 46 619.63 6.919 37 618.56 6.907 33 616.25 6.881 32 347.81 3.884 770 347.38 3.879 1000
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