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1,3-DIPHENOXYBENZENE

Product Name 1,3-DIPHENOXYBENZENE

CAS3379-38-2

MFC18H14O2

MW262.3

¹³CNMR

Mass

MS-IW-0059          
m-diphenoxybenzene
C18H14O2            (Mass of molecular ion:    262)

   Source Temperature: 260 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      39.0       2.2
      50.0       1.9
      51.0       8.4
      63.0       3.4
      64.0       4.2
      65.0       2.2
      75.0       1.1
      76.0       1.7
      77.0      15.0
      78.0       1.4
      89.0       1.0
      91.0       2.1
      92.0       1.8
      95.0       1.5
     115.0      18.9
     116.0       2.2
     121.0       5.3
     127.0       1.8
     128.0       4.7
     129.0       2.0
     131.0       1.5
     139.0       5.4
     140.0       4.1
     141.0      59.4
     142.0       7.6
     157.0       2.3
     168.0      14.1
     169.0      11.2
     170.0       1.4
     191.0       1.2
     193.0       1.0
     205.0       1.1
     215.0       1.6
     219.0       1.3
     233.0       3.0
     234.0       3.5
     261.0       4.3
     262.0     100.0
     263.0      19.6
     264.0       2.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₈ H₁₄ O₂	0.036 g : 0.5 ml CDCl₃
m-diphenoxybenzene

    Assign.     Shift(ppm)

      A             7.323
      B             7.237
      C             7.098
      D             7.025
      E             6.71
      F             6.69

     Hz     ppm     Int.

   2937.50   7.351     91
   2935.18   7.345    549
   2933.11   7.340    235
   2930.18   7.332    127
   2928.71   7.329    316
   2927.86   7.327    833
   2926.64   7.324    787
   2924.32   7.318    150
   2921.14   7.310    296
   2919.19   7.305    777
   2916.87   7.299    122
   2901.37   7.260    183
   2900.76   7.259    186
   2892.82   7.239    418
   2885.13   7.220    226
   2884.64   7.218    235
   2844.97   7.119    196
   2843.87   7.116    378
   2842.65   7.113    238
   2837.77   7.101    222
   2836.43   7.098    603
   2835.69   7.096    315
   2834.96   7.094    232
   2830.08   7.082    159
   2828.98   7.079    296
   2827.88   7.076    172
   2813.96   7.042    147
   2813.35   7.040    163
   2812.01   7.037    853
   2810.79   7.034   1000
   2810.06   7.032    568
   2808.72   7.028    281
   2805.30   7.020    272
   2804.32   7.017    464
   2803.22   7.015    855
   2802.25   7.012    756
   2799.68   7.006    112
   2688.23   6.727    567
   2685.91   6.721    623
   2680.42   6.707    220
   2679.69   6.706    272
   2677.86   6.701    814
   2674.44   6.692    364
   2672.61   6.688    397
   2670.29   6.682    165

in CDCl3

KBr disc

nujol mull

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