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MassMS-IW-1283 p-diphenoxybenzene C18H14O2 (Mass of molecular ion: 262)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 1.8 50.0 2.1 51.0 10.7 63.0 2.0 64.0 1.2 65.0 1.1 76.0 1.2 77.0 29.8 78.0 2.3 103.0 1.0 115.0 5.0 127.0 1.4 128.0 3.7 129.0 8.3 130.0 1.0 131.0 2.4 139.0 2.0 141.0 11.3 142.0 1.4 157.0 2.3 168.0 2.8 169.0 2.3 185.0 13.3 186.0 2.7 233.0 1.7 234.0 2.3 262.0 100.0 263.0 19.9 264.0 2.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C18 H14 O2 0.033 g : 0.5 ml CDCl3 p-diphenoxybenzene 
Assign. Shift(ppm)
A 7.322 B 7.079 C 7.00 D 6.995
Hz ppm Int.2935.06 7.345 125 2934.08 7.342 58 2932.86 7.339 49 2927.61 7.326 185 2926.39 7.323 176 2923.95 7.317 31 2920.90 7.309 63 2918.95 7.304 177 2837.16 7.100 44 2836.06 7.097 85 2834.96 7.094 52 2829.96 7.082 50 2828.74 7.079 133 2827.88 7.076 67 2827.27 7.075 52 2822.39 7.063 36 2821.29 7.060 65 2820.19 7.057 39 2804.32 7.017 34 2803.59 7.016 37 2802.25 7.012 191 2801.15 7.010 231 2800.42 7.008 122 2798.95 7.004 69 2795.65 6.996 1000 2793.58 6.991 227 2792.48 6.988 190 2789.92 6.981 33
in CDCl3
KBr disc
nujol mull
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