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MassMS-NW-1936 3-(3,4-dichlorophenyl)-1,1-dimethylurea C9H10Cl2N2O (Mass of molecular ion: 232)
Source Temperature: 190 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 5.5 18.0 3.9 28.0 3.2 42.0 4.3 43.0 1.6 44.0 11.1 45.0 4.3 56.0 1.7 61.0 1.3 62.0 2.1 63.0 2.0 72.0 100.0 73.0 4.0 74.0 1.3 75.0 1.1 88.0 1.5 97.0 1.7 109.0 1.1 124.0 7.3 125.0 1.4 126.0 2.5 133.0 1.5 159.0 3.4 160.0 1.1 161.0 3.0 187.0 11.7 188.0 1.1 189.0 7.4 191.0 1.3 232.0 16.5 233.0 1.9 234.0 10.5 235.0 1.0 236.0 1.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H10 Cl2 N2 O 0.046 g : 0.5 ml CDCl3 3-(3,4-dichlorophenyl)-1,1-dimethylurea 
Assign. Shift(ppm)
A 7.59 B 7.28 C 7.22 D 6.45 E 3.015
Hz ppm Int.680.94 7.604 111 680.15 7.595 119 679.36 7.586 121 650.79 7.267 277 647.86 7.234 140 270.01 3.015 1000
in CDCl3
KBr disc
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