SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List >  32953-14-3More Spectrum > N-Ethyl-3,4-(methylenedioxy)aniline(32953-14-3)IR1

32953-14-3

N-Ethyl-3,4-(methylenedioxy)aniline

Product Name N-Ethyl-3,4-(methylenedioxy)aniline

CAS32953-14-3

MFC9H11NO2

MW165.19

More

  • 32953-14-3_ms
    Mass

    MS-NW-7516          
    N-ethyl-3,4-methylenedioxyaniline
    C9H11NO2            (Mass of molecular ion:    165)
    

       Source Temperature: 250 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          26.0       1.1
          27.0       4.4
          28.0       5.3
          29.0       2.8
          38.0       1.5
          39.0       3.9
          40.0       1.0
          41.0       1.3
          42.0       1.3
          50.0       2.6
          51.0       8.1
          52.0       7.2
          53.0       3.5
          54.0       1.5
          62.0       2.4
          63.0       4.7
          64.0       1.9
          65.0       8.3
          66.0       1.3
          67.0       1.1
          68.0       1.7
          73.5       1.1
          74.5      10.7
          75.0       4.7
          77.0       2.8
          78.0      13.2
          79.0       4.9
          80.0       4.6
          81.5       2.1
          82.5       1.1
          91.0       1.5
          92.0       6.1
          93.0       4.8
          94.0       1.1
         104.0       1.1
         106.0       6.1
         107.0       2.4
         108.0       1.3
         120.0       7.3
         121.0       4.1
         122.0       6.3
         134.0       1.8
         136.0       5.4
         137.0       1.3
         148.0       2.7
         149.0       2.1
         150.0     100.0
         151.0      10.5
         152.0       1.1
         163.0       1.4
         164.0       5.7
         165.0      66.3
         166.0       7.0
         178.0       2.5
         193.0       1.3
    

90 MHz in CDCl3

  • 32953-14-3_1hnmr

    1H NMR 89.56 MHz
    C9 H11 N O2 0.05 ml : 0.5 ml CDCl3
    N-ethyl-3,4-methylenedioxyaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.614 B 6.210 C 6.008 D 5.792 E 3.15 F 3.060 G 1.190

         Hz     ppm     Int.
    

        597.31   6.670    140
        596.94   6.666    129
        589.06   6.578    187
        588.69   6.574    171
        557.13   6.221    132
        554.94   6.197    165
        542.75   6.061    123
        540.44   6.035     93
        534.50   5.969     90
        532.19   5.943     73
        518.75   5.793   1000
        284.19   3.174    110
        277.06   3.094    207
        269.94   3.015    209
        262.94   2.936     76
        113.38   1.266    239
        106.38   1.188    491
         99.19   1.108    199
         97.31   1.087     33
    

in CDCl3

liquid film