-
MS-NW-0022 ethyl formate C3H6O2 (Mass of molecular ion: 74)
Source Temperature: 200 °C Sample Temperature: 65 °C Reservoir, 75 eV
14.0 1.6 15.0 4.3 18.0 3.8 19.0 5.7 26.0 6.4 27.0 30.4 28.0 94.1 29.0 29.3 30.0 3.3 31.0 100.0 32.0 1.2 42.0 1.3 43.0 5.6 45.0 33.4 46.0 5.3 47.0 9.0 56.0 5.9 59.0 1.1 73.0 2.3 74.0 10.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C3 H6 O2 0.04 ml : 0.5 ml CDCl3 ethyl formate Assign. Shift(ppm)
A 8.026 B 4.215 C 1.289
Hz ppm Int.
720.75 8.048 53 719.31 8.032 372 718.69 8.025 390 718.06 8.018 215 717.00 8.006 96 388.81 4.342 108 388.19 4.335 113 381.69 4.262 422 380.88 4.253 429 374.56 4.183 450 373.75 4.174 445 367.44 4.103 126 366.75 4.096 131 122.94 1.373 429 122.31 1.366 475 115.88 1.294 891 115.25 1.287 1000 108.63 1.213 405 108.06 1.207 428
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