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MS-NW-6650 o-fluoroanisole C7H7FO (Mass of molecular ion: 126)
Source Temperature: 260 °C Sample Temperature: 180 °C Direct, 75 eV
15.0 2.1 28.0 1.3 29.0 1.1 31.0 3.1 37.0 1.5 38.0 2.6 39.0 3.7 50.0 4.4 51.0 3.1 56.0 2.5 57.0 17.6 61.0 1.5 62.0 1.9 63.0 4.9 64.0 1.8 68.0 1.9 69.0 2.8 70.0 1.4 74.0 2.2 75.0 7.4 76.0 1.0 77.0 2.3 81.0 4.0 82.0 3.1 83.0 60.4 84.0 3.4 92.0 1.2 94.0 1.2 95.0 6.8 96.0 8.6 97.0 6.6 111.0 52.6 112.0 4.2 125.0 1.5 126.0 100.0 127.0 7.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H7 F O 0.05 ml : 0.5 ml CDCl3 o-fluoroanisole Assign. Shift(ppm)
A 7.05 B 7.03 C 6.929 D 6.857 E 3.837
Hz ppm Int.
2826.29 7.072 86 2824.71 7.068 113 2821.41 7.060 52 2820.07 7.057 90 2818.36 7.053 112 2816.77 7.049 139 2814.70 7.043 99 2813.96 7.042 79 2812.99 7.039 241 2811.28 7.035 84 2810.42 7.033 78 2806.52 7.023 94 2804.93 7.019 209 2802.98 7.014 78 2777.95 6.951 88 2776.25 6.947 99 2769.65 6.931 137 2768.07 6.927 131 2766.48 6.923 41 2761.11 6.909 81 2759.40 6.905 51 2750.61 6.883 73 2749.02 6.879 70 2746.09 6.872 76 2744.51 6.868 69 2743.04 6.864 93 2741.46 6.860 79 2738.65 6.853 76 2737.92 6.851 72 2736.82 6.849 83 2735.11 6.844 57 2733.52 6.840 51 2730.59 6.833 50 2728.88 6.829 46 1533.45 3.837 1000
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