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2-Fluorobenzoyl chloride

Product Name 2-Fluorobenzoyl chloride

CAS393-52-2

MFC7H4ClFO

MW158.56

¹³CNMR

Mass

MS-NW-7784          
o-fluorobenzoyl chloride
C7H4ClFO            (Mass of molecular ion:    158)

   Source Temperature: 240 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      28.0       1.1
      31.0       1.5
      37.0       2.2
      38.0       1.7
      39.0       1.3
      47.5       2.2
      49.0       1.3
      50.0       6.8
      51.0       3.2
      57.0       1.1
      61.0       1.7
      61.5       6.4
      62.0       2.0
      63.0       1.3
      68.0       4.3
      69.0       5.3
      74.0       4.2
      75.0      18.6
      76.0       1.6
      93.0       1.4
      94.0       3.6
      95.0      40.1
      96.0       2.7
     123.0     100.0
     124.0       7.8
     158.0       4.0
     160.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₄ Cl F O	0.05 ml : 0.5 ml CDCl₃
o-fluorobenzoyl chloride

    Assign.     Shift(ppm)

      A             8.110
      B             7.680
      C             7.323
      D             7.197

     Hz     ppm     Int.

   3249.88   8.132    571
   3248.17   8.128    577
   3241.94   8.112    758
   3240.84   8.110    735
   3240.11   8.108    715
   3234.62   8.094    591
   3232.91   8.090    589
   3080.93   7.710    327
   3079.10   7.705    322
   3076.05   7.697    345
   3074.22   7.693    402
   3073.49   7.691    451
   3072.63   7.689    437
   3071.66   7.686    435
   3070.80   7.684    401
   3068.60   7.679    427
   3067.75   7.677    433
   3066.77   7.674    442
   3065.92   7.672    440
   3065.19   7.670    443
   3063.35   7.666    389
   3060.30   7.658    382
   3058.47   7.653    370
   2934.57   7.343    612
   2933.47   7.341    633
   2930.18   7.332     55
   2926.76   7.324    983
   2926.27   7.323   1000
   2925.66   7.321    947
   2919.07   7.305    525
   2918.09   7.302    537
   2915.16   7.295     32
   2886.23   7.222    650
   2885.13   7.220    617
   2877.81   7.201    621
   2876.71   7.199    611
   2875.37   7.195    676
   2874.27   7.192    638
   2866.94   7.174    588
   2865.84   7.171    568

in CDCl3

liquid film

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