-
MassMS-NW-9711 endo-2-norbornanamine hydrochloride C7H13N HCl (Mass of molecular ion: 111)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 2.3 27.0 2.9 28.0 7.9 29.0 1.7 30.0 16.2 35.0 3.0 36.0 29.8 37.0 1.1 38.0 10.5 39.0 6.9 40.0 1.4 41.0 8.8 42.0 7.4 43.0 33.6 44.0 7.8 45.0 15.6 51.0 1.5 52.0 1.0 53.0 3.6 54.0 3.7 55.0 3.1 56.0 50.3 57.0 14.3 65.0 5.1 66.0 17.3 67.0 17.5 68.0 5.0 69.0 12.9 70.0 27.7 71.0 1.4 77.0 5.3 78.0 2.5 79.0 56.9 80.0 7.0 81.0 3.1 82.0 100.0 83.0 18.6 84.0 1.0 91.0 3.1 93.0 4.7 94.0 47.6 95.0 4.4 96.0 10.7 110.0 8.7 111.0 45.9 112.0 4.9
400 MHz in CDCl3
-
1H NMR 399.65 MHz C7 H13 N 0.039 g : 0.5 ml CDCl3 endo-2-norbornanamine hydrochloride 
Assign. Shift(ppm)
A 8.43 B 3.561 C 2.61 D 2.297 E *1 2.052 F *2 1.86 G 1.60 J *2 1.55 K 1.42 L *1 1.260 ASSIGNED BY C-H COSY
Hz ppm Int.3368.41 8.429 403 1432.98 3.586 116 1428.96 3.576 229 1424.56 3.565 151 1422.49 3.560 158 1417.85 3.548 244 1413.94 3.538 138 1042.36 2.609 396 918.21 2.298 374 836.06 2.092 93 833.62 2.086 100 831.42 2.081 102 828.98 2.075 91 825.07 2.065 108 822.63 2.059 201 820.31 2.053 210 817.99 2.047 195 815.80 2.042 113 811.77 2.032 111 809.20 2.025 112 807.01 2.020 111 804.57 2.014 92 755.37 1.891 76 753.42 1.886 66 753.05 1.885 66 752.81 1.884 66 752.56 1.884 66 745.61 1.866 268 735.84 1.842 123 735.35 1.840 124 730.22 1.828 101 662.23 1.658 31 655.76 1.641 90 652.10 1.632 144 648.56 1.623 150 643.31 1.610 386 640.50 1.603 418 631.59 1.581 404 629.52 1.576 481 617.07 1.545 235 611.57 1.531 134 580.08 1.452 52 579.22 1.450 54 568.36 1.423 1000 557.86 1.396 72 556.27 1.392 78 513.06 1.284 183 510.99 1.279 200 509.03 1.274 206 506.96 1.269 180 503.17 1.260 36 499.63 1.251 173 497.56 1.245 188 495.61 1.241 195 493.65 1.236 169
in CDCl3
KBr disc
nujol mull
More Suppliers
