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MassMS-NW-5766 exo-2-aminonorbornane C7H13N (Mass of molecular ion: 111)
Source Temperature: 250 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.3 18.0 9.6 26.0 1.5 27.0 12.3 28.0 25.9 29.0 5.5 30.0 59.5 31.0 1.3 38.0 2.0 39.0 19.0 40.0 3.9 41.0 20.6 42.0 16.9 43.0 70.9 44.0 16.3 45.0 29.9 50.0 1.6 51.0 3.0 52.0 2.0 53.0 6.4 54.0 6.2 55.0 5.0 56.0 77.2 57.0 23.6 58.0 1.1 65.0 5.5 66.0 22.1 67.0 22.5 68.0 6.2 69.0 16.0 70.0 35.5 71.0 2.2 77.0 4.5 78.0 1.7 79.0 38.5 80.0 5.9 81.0 3.5 82.0 100.0 83.0 21.1 84.0 1.9 91.0 2.3 93.0 4.8 94.0 40.5 95.0 4.9 96.0 9.6 97.0 1.0 110.0 12.1 111.0 57.6 112.0 4.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H13 N 0.05 ml : 0.5 ml CDCl3 exo-2-aminonorbornane 
Assign. Shift(ppm)
A 2.805 B 2.207 C 1.925 D 1.633 E 1.46 to 1.42 F 1.09 G 1.06 J 1.05 K 1.01 ASSIGNED BY C-H COSY
Hz ppm Int.1126.59 2.819 323 1123.29 2.811 333 1119.02 2.800 345 1115.72 2.792 339 882.20 2.208 502 771.12 1.930 521 767.46 1.921 488 664.43 1.663 277 661.99 1.657 280 656.74 1.644 276 654.30 1.638 289 651.73 1.631 320 649.29 1.625 319 644.04 1.612 310 641.72 1.606 309 591.43 1.480 432 589.72 1.476 575 587.77 1.471 539 585.94 1.467 565 583.50 1.461 411 581.54 1.456 767 579.71 1.451 910 578.25 1.447 1000 576.05 1.442 717 574.34 1.438 923 570.19 1.427 645 566.77 1.419 483 565.55 1.416 508 562.74 1.409 417 444.34 1.112 474 442.99 1.109 540 441.89 1.106 586 440.67 1.103 474 434.45 1.088 409 433.11 1.084 586 432.01 1.081 748 430.66 1.078 590 423.83 1.061 791 421.88 1.056 739 416.87 1.044 571 414.79 1.038 572 405.03 1.014 377
in CDCl3
liquid film
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