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5,6-Dimethyl-1,10-phenanthroline

Product Name 5,6-Dimethyl-1,10-phenanthroline

CAS3002-81-1

MFC14H12N2

MW208.26

¹³CNMR

Mass

MS-KW-0504          
5,6-dimethyl-1,10-phenanthroline
C14H12N2            (Mass of molecular ion:    208)

   Source Temperature: 170 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      39.0       1.9
      50.0       1.3
      51.0       2.8
      62.0       1.0
      63.0       3.6
      64.0       1.0
      69.5       2.7
      75.0       2.6
      75.5       1.5
      76.0       4.6
      76.5       2.0
      77.0       4.2
      78.0       1.2
      82.5       3.4
      83.0       4.4
      83.5       1.1
      88.5       1.2
      89.0       4.4
      89.5       4.8
      90.0       4.5
      90.5       1.5
      91.0       1.3
      96.0       3.6
      96.5       4.3
     102.0       2.8
     102.5       1.1
     103.0       6.0
     103.5       1.6
     104.0       8.6
     104.5       1.3
     126.0       1.0
     127.0       1.7
     138.0       1.0
     139.0       2.1
     140.0       2.4
     151.0       2.5
     152.0       4.0
     153.0       1.8
     154.0       1.7
     164.0       2.3
     165.0       2.4
     166.0       4.7
     167.0       2.9
     168.0       1.1
     177.0       1.4
     178.0       2.9
     179.0       3.2
     180.0       4.3
     181.0       3.2
     191.0       2.1
     192.0      14.1
     193.0      86.7
     194.0      12.9
     195.0       1.0
     205.0       9.3
     206.0       4.2
     207.0      20.8
     208.0     100.0
     209.0      16.2
     210.0       1.2

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₁₂ N₂	0.030 g : 0.5 ml CDCl₃
5,6-dimethyl-1,10-phenanthroline

    Assign.     Shift(ppm)

      A             9.091
      B             8.305
      C             7.557
      D             2.574
     
     J(A,B)=1.7HZ. J(A,C)=4.3HZ. J(B,C)=8.4HZ.

     Hz     ppm     Int.

    817.25   9.126     78
    815.56   9.107     85
    812.94   9.078     84
    811.31   9.059     90
    749.31   8.367     72
    747.69   8.349     73
    740.94   8.274     93
    739.25   8.255     89
    682.69   7.623    128
    678.38   7.575    121
    674.25   7.529    103
    670.00   7.482     97
    230.56   2.575   1000

in CDCl3

KBr disc

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