5,6-Dimethyl-1,10-phenanthroline

Mass

MS-KW-0504          
5,6-dimethyl-1,10-phenanthroline
C14H12N2            (Mass of molecular ion:    208)

   Source Temperature: 170 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      39.0       1.9
      50.0       1.3
      51.0       2.8
      62.0       1.0
      63.0       3.6
      64.0       1.0
      69.5       2.7
      75.0       2.6
      75.5       1.5
      76.0       4.6
      76.5       2.0
      77.0       4.2
      78.0       1.2
      82.5       3.4
      83.0       4.4
      83.5       1.1
      88.5       1.2
      89.0       4.4
      89.5       4.8
      90.0       4.5
      90.5       1.5
      91.0       1.3
      96.0       3.6
      96.5       4.3
     102.0       2.8
     102.5       1.1
     103.0       6.0
     103.5       1.6
     104.0       8.6
     104.5       1.3
     126.0       1.0
     127.0       1.7
     138.0       1.0
     139.0       2.1
     140.0       2.4
     151.0       2.5
     152.0       4.0
     153.0       1.8
     154.0       1.7
     164.0       2.3
     165.0       2.4
     166.0       4.7
     167.0       2.9
     168.0       1.1
     177.0       1.4
     178.0       2.9
     179.0       3.2
     180.0       4.3
     181.0       3.2
     191.0       2.1
     192.0      14.1
     193.0      86.7
     194.0      12.9
     195.0       1.0
     205.0       9.3
     206.0       4.2
     207.0      20.8
     208.0     100.0
     209.0      16.2
     210.0       1.2

Assign. Shift(ppm) A 9.091 B 8.305 C 7.557 D 2.574 J(A,B)=1.7HZ. J(A,C)=4.3HZ. J(B,C)=8.4HZ.

     Hz     ppm     Int.

    817.25   9.126     78
    815.56   9.107     85
    812.94   9.078     84
    811.31   9.059     90
    749.31   8.367     72
    747.69   8.349     73
    740.94   8.274     93
    739.25   8.255     89
    682.69   7.623    128
    678.38   7.575    121
    674.25   7.529    103
    670.00   7.482     97
    230.56   2.575   1000