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MassMS-NW-5889 2,3-dimethylanisole C9H12O (Mass of molecular ion: 136)
Source Temperature: 280 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.5 27.0 4.0 38.0 1.3 39.0 8.6 40.0 1.0 41.0 3.0 50.0 2.2 51.0 5.9 52.0 2.6 53.0 3.4 62.0 1.1 63.0 3.2 65.0 6.5 66.0 1.0 67.0 1.2 77.0 21.9 78.0 7.1 79.0 4.4 89.0 1.1 91.0 31.2 92.0 3.5 93.0 6.5 103.0 6.4 104.0 4.4 105.0 14.5 106.0 3.8 107.0 3.2 121.0 66.9 122.0 8.9 135.0 8.6 136.0 100.0 137.0 10.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H12 O 0.05 ml : 0.5 ml CDCl3 2,3-dimethylanisole 
Assign. Shift(ppm)
A 7.027 B 6.751 C 6.670 D 3.757 E 2.242 F 2.133
Hz ppm Int.2817.02 7.049 77 2809.08 7.029 151 2801.15 7.010 95 2701.66 6.761 133 2694.09 6.742 117 2669.68 6.681 132 2661.38 6.660 118 1501.71 3.758 1000 896.00 2.242 694 888.67 2.224 29 852.54 2.134 709
in CDCl3
liquid film
4880 A,200 M,liquid
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