2-BIPHENYLMETHANOL

Mass

MS-NW-8773          
2-biphenylmethanol
C13H12O             (Mass of molecular ion:    184)

   Source Temperature: 280 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       2.2
      27.0       1.6
      28.0       1.5
      39.0       3.8
      50.0       2.6
      51.0       8.8
      52.0       1.8
      55.0       1.4
      62.0       1.5
      63.0       5.8
      64.0       2.6
      65.0       1.9
      69.5       2.5
      74.0       2.2
      75.0       3.4
      75.5       1.0
      76.0       9.7
      76.5       1.7
      77.0      20.2
      78.0      11.3
      79.0       8.3
      81.0       1.1
      81.5       1.8
      82.0       6.7
      82.5       7.9
      83.0       5.0
      87.0       1.5
      89.0       2.8
      90.0       1.2
      91.0       6.3
      91.5       2.2
      92.0       2.2
     101.0       1.4
     102.0       2.7
     103.0       1.1
     105.0       9.7
     106.0       2.0
     107.0       8.2
     113.0       1.0
     115.0      11.7
     116.0       2.4
     118.0       1.8
     126.0       3.1
     127.0       5.8
     128.0       9.0
     129.0       5.5
     130.0       1.5
     139.0       4.0
     141.0       7.8
     142.0       1.6
     143.0       1.2
     150.0       2.4
     151.0       6.9
     152.0      23.5
     153.0      16.3
     154.0       7.5
     155.0      43.5
     156.0      10.0
     157.0       1.8
     163.0       3.2
     164.0       4.8
     165.0      78.5
     166.0      67.7
     167.0      17.6
     168.0       3.1
     169.0       8.8
     170.0       1.2
     181.0       5.6
     182.0       2.3
     183.0      22.3
     184.0     100.0
     185.0      14.1
     186.0       1.1

Assign. Shift(ppm) A 7.52 B 7.40 C 7.35 D 7.34 E 7.33 F 7.268 G 4.576 J 1.80 ASSIGNED BY H-H AND C-H COSY. CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

   3012.45   7.538    187
   3011.96   7.537    197
   3010.25   7.533    248
   3006.23   7.523     93
   3005.49   7.521    170
   3004.64   7.519    198
   3004.03   7.517    192
   3003.42   7.516    256
   3002.93   7.514    244
   2971.44   7.436     35
   2971.07   7.435     36
   2970.09   7.432     41
   2968.99   7.429     58
   2967.77   7.426    149
   2966.19   7.422    208
   2964.97   7.419    127
   2964.48   7.418    138
   2961.79   7.411    168
   2960.57   7.408    303
   2958.74   7.404    341
   2958.25   7.403    310
   2957.40   7.400    367
   2956.18   7.397    161
   2955.08   7.395    207
   2952.15   7.387    685
   2951.42   7.386    732
   2950.07   7.382    232
   2946.17   7.372    418
   2944.21   7.367    546
   2942.87   7.364    490
   2939.94   7.357    563
   2939.21   7.355    976
   2938.48   7.353   1000
   2937.74   7.351    758
   2937.13   7.350    810
   2936.16   7.347    552
   2932.74   7.339    559
   2931.15   7.335    654
   2929.57   7.331    420
   2928.22   7.327    138
   2927.37   7.325     96
   2925.29   7.320    178
   2923.58   7.316    142
   2920.90   7.309     33
   2919.92   7.307     39
   2918.09   7.302     34
   2915.04   7.294     33
   2914.43   7.293     31
   2912.35   7.288     34
   2908.81   7.279    321
   2907.35   7.275    250
   2906.37   7.273    211
   2901.73   7.261    293
   2899.66   7.256    185
   1828.86   4.577    798
    718.75   1.799    220