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MS-IW-1366 9-fluorenol C13H10O (Mass of molecular ion: 182)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
63.0 1.2 76.0 3.8 77.0 1.2 90.5 1.7 91.0 1.4 126.0 1.4 127.0 1.3 139.0 1.0 150.0 2.6 151.0 7.2 152.0 24.8 153.0 19.0 154.0 2.8 163.0 3.9 164.0 3.0 165.0 12.6 166.0 4.0 180.0 7.3 181.0 100.0 182.0 90.1 183.0 12.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H10 O 18.0 mg : 0.5 ml CDCl3 9-fluorenol Assign. Shift(ppm)
A 7.62 B 7.61 C 7.370 D 7.303 E 5.521 F 1.98 J(E,F)=10.0HZ.
Hz ppm Int.
3050.42 7.633 555 3046.88 7.624 86 3046.26 7.623 81 3043.21 7.615 980 3042.48 7.613 1000 3035.03 7.595 569 3034.55 7.594 554 3033.94 7.592 525 3033.20 7.590 290 2954.10 7.392 223 2953.61 7.391 229 2952.88 7.389 247 2946.66 7.374 526 2946.17 7.372 538 2945.43 7.371 550 2939.21 7.355 350 2938.72 7.354 346 2937.99 7.352 335 2925.42 7.320 516 2924.19 7.317 527 2921.88 7.312 63 2917.97 7.302 728 2916.87 7.299 679 2910.64 7.283 287 2909.42 7.280 273 2211.79 5.535 284 2201.66 5.509 290 796.51 1.994 698 786.50 1.968 704
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