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9-Fluorenol

Product Name 9-Fluorenol

CAS1689-64-1

MFC13H10O

MW182.22

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  • Mass 

    MS-IW-1366          
9-fluorenol
C13H10O             (Mass of molecular ion:    182)


       Source Temperature: 150 °C
   Sample Temperature: 110 °C
   Direct, 75 eV


          63.0       1.2
      76.0       3.8
      77.0       1.2
      90.5       1.7
      91.0       1.4
     126.0       1.4
     127.0       1.3
     139.0       1.0
     150.0       2.6
     151.0       7.2
     152.0      24.8
     153.0      19.0
     154.0       2.8
     163.0       3.9
     164.0       3.0
     165.0      12.6
     166.0       4.0
     180.0       7.3
     181.0     100.0
     182.0      90.1
     183.0      12.1

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C13 H10 O 18.0 mg : 0.5 ml CDCl3
    9-fluorenol
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.62
      B             7.61
      C             7.370
      D             7.303
      E             5.521
      F             1.98
     
     J(E,F)=10.0HZ.
  

         Hz     ppm     Int.


       3050.42   7.633    555
   3046.88   7.624     86
   3046.26   7.623     81
   3043.21   7.615    980
   3042.48   7.613   1000
   3035.03   7.595    569
   3034.55   7.594    554
   3033.94   7.592    525
   3033.20   7.590    290
   2954.10   7.392    223
   2953.61   7.391    229
   2952.88   7.389    247
   2946.66   7.374    526
   2946.17   7.372    538
   2945.43   7.371    550
   2939.21   7.355    350
   2938.72   7.354    346
   2937.99   7.352    335
   2925.42   7.320    516
   2924.19   7.317    527
   2921.88   7.312     63
   2917.97   7.302    728
   2916.87   7.299    679
   2910.64   7.283    287
   2909.42   7.280    273
   2211.79   5.535    284
   2201.66   5.509    290
    796.51   1.994    698
    786.50   1.968    704

in CDCl3



KBr disc



nujol mull





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