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29022-11-5

Fmoc-Gly-OH

Product Name Fmoc-Gly-OH

CAS29022-11-5

MFC17H15NO4

MW297.31

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  • 29022-11-5_ms
    Mass

    MS-IW-2646          
    N-((9-fluorenyl)methoxycarbonyl)glycine
    C17H15NO4           (Mass of molecular ion:    297)
    

       Source Temperature: 180 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          28.0       4.4
          29.0       6.2
          30.0       1.5
          44.0       1.8
          56.0       2.1
          57.0       3.1
          63.0       2.5
          69.5       1.3
          74.0       1.8
          75.0       1.6
          76.0       2.4
          81.5       1.2
          82.0       1.1
          82.5       1.9
          87.0       1.5
          88.0       2.3
          89.0       3.3
         101.0       3.9
         115.0       3.1
         126.0       1.2
         139.0       5.0
         150.0       1.1
         151.0       1.9
         152.0       2.8
         162.0       1.3
         163.0      11.0
         164.0      10.0
         165.0     100.0
         166.0      74.9
         167.0      10.4
         176.0       4.3
         177.0       3.4
         178.0      55.4
         179.0      10.4
         180.0       1.0
         196.0      30.8
         197.0       4.8
         297.0       1.3
    

400 MHz in DMSO-d6

  • 29022-11-5_1hnmr

    1H NMR 399.65 MHz
    C17 H15 N O4 0.050 g : 0.5 ml DMSO-d6
    N-((9-fluorenyl)methoxycarbonyl)glycine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.900 B 7.734 C 7.67 D 7.429 E 7.348 F 4.325 G 4.252 J 3.704 J(C,J)=6.2HZ

         Hz     ppm     Int.
    

       3161.13   7.910    914
       3153.69   7.892   1000
       3145.51   7.871     31
       3145.26   7.871     31
       3094.73   7.744    727
       3087.40   7.726    816
       3079.35   7.706     40
       3078.61   7.704     39
       3077.76   7.702     41
       3077.27   7.700     42
       3077.03   7.700     42
       3076.78   7.699     42
       3076.05   7.697     40
       3075.44   7.696     37
       3074.83   7.694     38
       3073.85   7.692     40
       3073.36   7.691     42
       3069.09   7.680    190
       3062.99   7.665    422
       3056.88   7.649    225
       2977.05   7.450    426
       2969.73   7.431    963
       2962.16   7.412    606
       2955.44   7.396     41
       2954.59   7.393     37
       2952.88   7.389     31
       2951.42   7.386     34
       2950.56   7.383     34
       2950.20   7.382     33
       2947.39   7.375    108
       2943.36   7.365    586
       2939.94   7.357    239
       2938.72   7.354    272
       2935.91   7.347    875
       2929.32   7.330    355
       2928.47   7.328    373
       1744.51   4.366     32
       1744.14   4.365     32
       1743.53   4.363     33
       1742.68   4.361     31
       1742.31   4.360     32
       1741.70   4.359     32
       1740.97   4.357     35
       1732.67   4.336    561
       1725.83   4.319    958
       1718.38   4.300     72
       1717.04   4.297     67
       1715.70   4.294     59
       1714.97   4.292     58
       1714.60   4.291     56
       1713.99   4.289     54
       1713.26   4.287     53
       1712.65   4.286     52
       1711.67   4.283     51
       1711.18   4.282     52
       1705.32   4.268    301
       1698.73   4.251    382
       1698.36   4.250    383
       1692.02   4.234    193
       1685.67   4.218     48
       1684.20   4.215     40
       1683.47   4.213     38
       1682.98   4.212     36
       1682.37   4.210     34
       1682.01   4.209     34
       1681.27   4.207     32
       1680.54   4.206     31
       1680.05   4.204     30
       1503.17   3.762     31
       1502.20   3.759     32
       1501.59   3.758     33
       1500.24   3.754     36
       1499.63   3.753     38
       1499.02   3.751     39
       1497.44   3.747     44
       1497.07   3.746     45
       1496.46   3.745     47
       1495.61   3.743     50
       1495.24   3.742     51
       1494.75   3.741     53
       1494.02   3.739     56
       1493.29   3.737     60
       1492.68   3.735     62
       1492.31   3.735     64
       1491.58   3.733     67
       1490.60   3.730     71
       1483.64   3.713    815
       1477.42   3.697    822
       1469.48   3.677     55
       1468.14   3.674     49
       1466.80   3.671     42
       1466.19   3.669     40
       1465.70   3.668     38
       1465.09   3.666     35
       1464.48   3.665     34
       1462.77   3.661     30
    

in DMSO-d6

  • 29022-11-5_13cnmr

KBr disc

  • 29022-11-5_ir1_2

nujol mull

  • 29022-11-5_ir2