GLUTARYL DICHLORIDE

Mass

MS-NW-2637          
glutaryl dichloride
C5H6Cl2O2           (Mass of molecular ion:    168)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      14.0       3.9
      15.0       3.5
      18.0       1.7
      25.0       1.1
      26.0       7.5
      27.0      32.2
      28.0      16.8
      29.0       2.2
      32.0       3.3
      34.0       1.7
      35.0       3.5
      36.0      18.2
      37.0       3.4
      38.0       6.0
      39.0      32.3
      40.0       6.2
      41.0      80.6
      42.0      61.2
      43.0       4.4
      44.0       2.8
      49.0       5.7
      50.0       1.0
      51.0       1.6
      53.0       1.1
      55.0     100.0
      56.0       3.6
      61.0       1.1
      63.0      21.9
      65.0       7.3
      68.0       5.8
      69.0       6.8
      70.0       6.1
      75.0       1.5
      76.0       7.1
      77.0      21.3
      78.0       4.4
      79.0       6.8
      91.0       1.6
      96.0       2.5
      97.0      27.3
      98.0       1.6
     104.0      26.0
     105.0      40.9
     106.0      10.0
     107.0      13.3
     132.0       6.5
     133.0      62.6
     134.0       5.6
     135.0      21.0
     136.0       1.3

Assign. Shift(ppm) A 3.02 B 2.08

     Hz     ppm     Int.

    279.56   3.122     87
    278.94   3.115    227
    278.31   3.108    251
    271.81   3.035    570
    271.31   3.030   1000
    264.81   2.957    356
    264.31   2.952    336
    200.44   2.239     53
    199.38   2.227     58
    193.50   2.161    162
    192.94   2.155    174
    191.94   2.144     89
    186.44   2.082    211
    185.88   2.076    240
    185.00   2.066     66
    179.38   2.003    125
    178.81   1.997    137
    177.63   1.984     38
    172.31   1.924     31
    171.19   1.912     32