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MassMS-NW-2637 glutaryl dichloride C5H6Cl2O2 (Mass of molecular ion: 168)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
14.0 3.9 15.0 3.5 18.0 1.7 25.0 1.1 26.0 7.5 27.0 32.2 28.0 16.8 29.0 2.2 32.0 3.3 34.0 1.7 35.0 3.5 36.0 18.2 37.0 3.4 38.0 6.0 39.0 32.3 40.0 6.2 41.0 80.6 42.0 61.2 43.0 4.4 44.0 2.8 49.0 5.7 50.0 1.0 51.0 1.6 53.0 1.1 55.0 100.0 56.0 3.6 61.0 1.1 63.0 21.9 65.0 7.3 68.0 5.8 69.0 6.8 70.0 6.1 75.0 1.5 76.0 7.1 77.0 21.3 78.0 4.4 79.0 6.8 91.0 1.6 96.0 2.5 97.0 27.3 98.0 1.6 104.0 26.0 105.0 40.9 106.0 10.0 107.0 13.3 132.0 6.5 133.0 62.6 134.0 5.6 135.0 21.0 136.0 1.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H6 Cl2 O2 0.05 ml : 0.5 ml CDCl3 glutaryl dichloride 
Assign. Shift(ppm)
A 3.02 B 2.08
Hz ppm Int.279.56 3.122 87 278.94 3.115 227 278.31 3.108 251 271.81 3.035 570 271.31 3.030 1000 264.81 2.957 356 264.31 2.952 336 200.44 2.239 53 199.38 2.227 58 193.50 2.161 162 192.94 2.155 174 191.94 2.144 89 186.44 2.082 211 185.88 2.076 240 185.00 2.066 66 179.38 2.003 125 178.81 1.997 137 177.63 1.984 38 172.31 1.924 31 171.19 1.912 32
in CDCl3
liquid film
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