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28009-80-5

DI-TERT-BUTYL 1,3-ACETONEDICARBOXYLATE

Product Name DI-TERT-BUTYL 1,3-ACETONEDICARBOXYLATE

CAS28009-80-5

MFC13H22O5

MW258.31

  • 28009-80-5_ms_1
    Mass

    MS-NW-7524          
    di-tert-butyl 3-oxoglutarate
    C13H22O5            (Mass of molecular ion:    258)
    

       Source Temperature: 230 °C
       Sample Temperature: 170 °C
       Reservoir, 75 eV
    

          15.0       1.7
          27.0       3.5
          28.0       2.0
          29.0      11.4
          31.0       4.9
          39.0       4.5
          41.0      20.4
          42.0       4.4
          43.0      10.6
          44.0       4.5
          55.0       2.2
          56.0       7.4
          57.0     100.0
          58.0       4.7
          59.0      28.1
          60.0       1.1
          69.0       2.6
          84.0       1.6
          85.0       1.7
          87.0       1.5
         102.0       8.2
         103.0       1.5
         111.0       2.8
         115.0       1.7
         128.0       1.5
         129.0       7.9
         146.0       1.9
         147.0      12.2
    

parameter in CDCl3

  • 28009-80-5_1hnmr_1

    1H NMR 300 MHz
    C13 H22 O5 0.040 g : 0.5 ml CDCl3
    di-tert-butyl 3-oxoglutarate
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 3.496 D(B) 1.473

         Hz     ppm     Int.
    

       1048.80   3.496    222
        441.91   1.473   1000
    

in CDCl3

  • 28009-80-5_13cnmr_1

KBr disc

  • 28009-80-5_ir1_2

nujol mull

  • 28009-80-5_ir2_1

  • 28009-80-5_raman