Dimethyl chlorothiophosphate

Mass

MS-NW-4878          
O,O'-dimethyl chlorothiophosphate
C2H6ClO2PS          (Mass of molecular ion:    160)

   Source Temperature: 270 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      14.0       1.9
      15.0      28.0
      18.0       1.2
      28.0       2.9
      29.0       8.9
      30.0       1.5
      31.0       8.0
      32.0       2.3
      33.0       1.3
      36.0       2.1
      44.0       1.5
      45.0       9.4
      46.0       6.5
      47.0      54.9
      48.0       4.3
      49.0       4.0
      50.0      11.5
      52.0       3.8
      61.0       2.1
      62.0       5.3
      63.0      23.7
      64.0       7.0
      65.0       1.3
      66.0       2.5
      67.0       2.5
      76.0       1.5
      77.0       4.7
      79.0      19.7
      80.0       2.9
      81.0       1.1
      83.0       1.6
      93.0      13.3
      94.0       6.7
      95.0       1.9
      96.0       1.3
      97.0      99.9
      98.0       2.9
      99.0      33.0
     100.0       1.4
     110.0       1.2
     111.0       1.1
     113.0       7.4
     114.0       1.9
     115.0       4.2
     116.0       1.2
     125.0      48.6
     126.0       2.0
     127.0       2.7
     129.0      17.1
     130.0      92.4
     131.0       8.2
     132.0      36.0
     133.0       1.3
     134.0       1.7
     141.0       2.0
     142.0       1.0
     145.0       4.2
     146.0       2.1
     147.0       1.8
     157.0       5.0
     160.0     100.0
     161.0       3.7
     162.0      37.8
     163.0       1.3
     164.0       1.8
     176.0       2.3
     180.0       1.9
     182.0       1.3
     192.0       4.5
     194.0       2.1
     204.0       1.9

Assign. Shift(ppm) A 3.907 J(A,P-31)=16.0HZ

     Hz     ppm     Int.

    357.88   3.996   1000
    356.63   3.983     34
    355.56   3.971     23
    341.88   3.818    999
    340.63   3.804     38