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MassMS-IW-7579 (1-pyrenyl)methanol C17H12O (Mass of molecular ion: 232)
Source Temperature: 170 °C Sample Temperature: 150 °C Direct, 75 eV
17.0 1.2 18.0 6.7 87.0 2.0 88.0 2.4 93.5 3.0 94.0 1.5 94.5 6.2 95.0 1.6 99.0 1.4 99.5 1.4 100.0 8.1 100.5 4.0 101.0 7.2 101.5 1.5 102.0 2.9 105.5 2.2 106.0 2.1 106.5 6.6 107.0 4.0 107.5 3.2 108.0 3.0 115.5 4.1 116.0 2.5 174.0 1.1 187.0 1.7 189.0 5.0 198.0 1.5 199.0 2.0 200.0 10.9 201.0 14.6 202.0 31.7 203.0 47.0 204.0 9.8 211.0 1.9 212.0 1.2 213.0 8.9 214.0 4.8 215.0 50.2 216.0 30.7 217.0 5.1 229.0 5.4 230.0 8.7 231.0 14.3 232.0 100.0 233.0 18.3 234.0 1.9
400 MHz at 60C
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1H NMR 399.65 MHz C17 H12 O saturated in CDCl3 at 60 C (1-pyrenyl)methanol 
Assign. Shift(ppm)
A 8.194 B 8.080 C 7.994 D 7.983 E 7.93 F 7.92 G 7.90 J 5.241 K 1.90
Hz ppm Int.3279.91 8.207 388 3270.75 8.185 488 3233.40 8.091 654 3229.98 8.083 45 3229.49 8.081 46 3225.71 8.072 786 3199.71 8.007 322 3194.58 7.994 497 3192.02 7.988 491 3187.99 7.977 37 3185.42 7.971 393 3179.20 7.955 186 3170.29 7.933 1000 3165.41 7.921 798 3163.57 7.916 458 3162.96 7.915 465 3158.08 7.903 501 3156.74 7.899 323 3155.64 7.897 382 3150.27 7.883 344 2094.73 5.242 802 760.01 1.902 222
in CDCl3
KBr disc
nujol mull
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