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MS-NW-8797 m-terphenyl-2'-ol C18H14O (Mass of molecular ion: 246)
Source Temperature: 160 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.2 77.0 1.1 89.0 1.1 94.5 2.1 101.0 1.6 107.0 1.1 107.5 1.8 108.0 1.1 115.0 3.3 123.0 3.1 139.0 1.8 141.0 1.2 168.0 1.5 169.0 1.5 189.0 1.6 202.0 7.8 203.0 3.5 213.0 1.2 215.0 7.1 216.0 2.6 217.0 7.1 218.0 4.2 226.0 3.6 227.0 5.5 228.0 1.4 231.0 1.0 244.0 1.7 245.0 18.1 246.0 100.0 247.0 19.4 248.0 2.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C18 H14 O 0.040 g : 0.5 ml CDCl3 m-terphenyl-2'-ol Assign. Shift(ppm)
A 7.541 B 7.454 C 7.365 D 7.262 E 7.042 F 5.38
Hz ppm Int.
3020.02 7.557 581 3018.55 7.553 762 3016.48 7.548 233 3012.57 7.539 447 3011.60 7.536 938 3010.86 7.534 679 3010.25 7.533 799 3008.42 7.528 149 2987.30 7.475 184 2986.45 7.473 373 2985.72 7.471 566 2983.89 7.467 212 2979.86 7.457 266 2978.39 7.453 1000 2977.05 7.450 422 2972.17 7.437 263 2970.70 7.434 464 2968.75 7.429 103 2950.68 7.384 237 2949.22 7.380 428 2947.88 7.377 245 2945.56 7.371 40 2943.97 7.367 182 2941.89 7.362 429 2939.70 7.356 145 2935.91 7.347 121 2934.57 7.343 204 2933.23 7.340 108 2906.62 7.273 732 2903.32 7.265 36 2902.34 7.263 40 2899.05 7.254 880 2821.41 7.060 355 2814.21 7.042 344 2813.48 7.040 315 2806.27 7.022 260 2149.90 5.380 858
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